(S)-2-(2-hydroxybenzylamino)-3-carbamoylpropanoic acid

Base Information

• Chemical Name: (S)-2-(2-hydroxybenzylamino)-3-carbamoylpropanoic acid
• CAS No.: 1164135-82-3
• Molecular Formula: C₁₁H₁₄N₂O₄
• Molecular Weight: 238.243

Synonyms:(S)-2-(2-hydroxybenzylamino)-3-carbamoylpropanoic acid

Chemical Property of (S)-2-(2-hydroxybenzylamino)-3-carbamoylpropanoic acid

Chemical Property:

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Technology Process of (S)-2-(2-hydroxybenzylamino)-3-carbamoylpropanoic acid

There total 2 articles about (S)-2-(2-hydroxybenzylamino)-3-carbamoylpropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C11H12N2O4 (63546-35-0) → (S)-2-(2-hydroxybenzylamino)-3-carbamoylpropanoic acid (1164135-82-3)

Guidance literature:

With sodium tetrahydroborate; In ethanol; water; Cooling with ice;

DOI:10.1002/anie.200900838

Reference yield:

C11H12N2O4 → (R)-2-(2-hydroxybenzylamino)-3-carbamoylpropanoic acid (1164135-82-3)

Guidance literature:

With sodium tetrahydroborate; In ethanol; water; Cooling with ice;

DOI:10.1002/anie.200900838

Reference yield: 82.0%

nickel(II) nitrate hexahydrate + (S)-2-(2-hydroxybenzylamino)-3-carbamoylpropanoic acid (1164135-82-3) → [Ni(II)(N-(2-hydroxybenzyl)-L-aspargine(-1H))2]

Guidance literature:

In water; satd. aq. soln. of Ni salt slowly diffused into satd. aq. soln. of ligand for a wk; crystals obtained; elem. anal.;

DOI:10.1016/j.ica.2008.12.018

upstream raw materials:

C₁₁H₁₂N₂O₄

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