C₄₁H₅₈O₁₀

Base Information

Chemical Name:C₄₁H₅₈O₁₀
CAS No.:1011242-84-4
Molecular Formula:C₄₁H₅₈O₁₀
Molecular Weight:710.906
Hs Code.:

C<sub>41</sub>H<sub>58</sub>O<sub>10</sub>

Synonyms:C₄₁H₅₈O₁₀

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Chemical Property of C₄₁H₅₈O₁₀

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Technology Process of C₄₁H₅₈O₁₀

There total 19 articles about C₄₁H₅₈O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1011242-82-2
C₄₅H₅₉BrN₂O₁₁S

: 1011242-84-4
C₄₁H₅₈O₁₀

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; In 1,4-dioxane; for 5h; Heating;
DOI:10.1021/jo7024515

Reference yield:

: C₂₅H₃₁IO₃Si

: 1011242-84-4
C₄₁H₅₈O₁₀

Guidance literature:: Multi-step reaction with 10 steps

1.1: Tetrabutylammoniumsalz der Diphenylphosphinsaeure; copper(I) thiophene-2-carboxylate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere; Schlenk technique

2.1: tributylphosphine / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C

4.1: manganese(IV) oxide / dichloromethane / 5 h / 20 °C

5.1: (2R,5R)-(+)-2-tert-butyl-3-methyl-5-benzyl-4-imidazolidinone; trifluoroacetic acid / water; acetonitrile / 72 h / -20 °C

6.1: n-butyllithium / tetrahydrofuran / 0.67 h / -78 °C

6.2: 2 h / -78 °C

6.3: 20 h / -78 - 20 °C

7.1: silver(I) triflimide; [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I); N-iodo-succinimide / acetone; water / 5 h / -15 - 20 °C

8.1: palladium diacetate; tetraethylammonium chloride; trifuran-2-yl-phosphane / toluene / 6 h / 90 °C / 2280.15 Torr / Molecular sieve

9.1: pyridine; hydrogen fluoride / tetrahydrofuran / 0 - 20 °C

10.1: dichloromethane / 1 h / 20 °C / Molecular sieve

10.2: 24 h / -30 °C

With pyridine; (2R,5R)-(+)-2-tert-butyl-3-methyl-5-benzyl-4-imidazolidinone; manganese(IV) oxide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-iodo-succinimide; n-butyllithium; copper(I) thiophene-2-carboxylate; trifuran-2-yl-phosphane; [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I); tributylphosphine; hydrogen fluoride; tetraethylammonium chloride; palladium diacetate; diisobutylaluminium hydride; Tetrabutylammoniumsalz der Diphenylphosphinsaeure; trifluoroacetic acid; silver(I) triflimide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; 1.1: |Stille Cross Coupling / 5.1: |Diels-Alder Cycloaddition / 6.1: |Corey-Fuchs Alkyne Synthesis / 6.2: |Corey-Fuchs Alkyne Synthesis;
DOI:10.1021/jacs.6b07585

Reference yield:

: 779338-03-3
C₁₈H₂₉NO₅

: 1011242-84-4
C₄₁H₅₈O₁₀

Guidance literature:: Multi-step reaction with 10 steps

1.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C

2.1: (1S,2R)-(-)-2-(N,N-di-n-butylamino)-1-phenylpropan-1-ol / toluene; hexane / 24 h / 0 °C

3.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / 0 °C

4.1: diisobutylaluminium hydride / tetrahydrofuran / 2 h / -78 °C

5.1: triphenylphosphine / dichloromethane / 0.5 h / -15 °C

5.2: 1 h / -20 °C

6.1: n-butyllithium / tetrahydrofuran / 0.67 h / -78 °C

6.2: 2 h / -78 °C

6.3: 20 h / -78 - 20 °C

7.1: silver(I) triflimide; [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I); N-iodo-succinimide / acetone; water / 5 h / -15 - 20 °C

8.1: palladium diacetate; tetraethylammonium chloride; trifuran-2-yl-phosphane / toluene / 6 h / 90 °C / 2280.15 Torr / Molecular sieve

9.1: pyridine; hydrogen fluoride / tetrahydrofuran / 0 - 20 °C

10.1: dichloromethane / 1 h / 20 °C / Molecular sieve

10.2: 24 h / -30 °C

With pyridine; 2,6-dimethylpyridine; N-iodo-succinimide; n-butyllithium; trifuran-2-yl-phosphane; [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I); hydrogen fluoride; tetraethylammonium chloride; palladium diacetate; sulfur trioxide pyridine complex; diisobutylaluminium hydride; (1S,2R)-(-)-2-(N,N-di-n-butylamino)-1-phenylpropan-1-ol; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; silver(I) triflimide; In tetrahydrofuran; hexane; dichloromethane; water; acetone; toluene; 6.1: |Corey-Fuchs Alkyne Synthesis / 6.2: |Corey-Fuchs Alkyne Synthesis;
DOI:10.1021/jacs.6b07585