4-(tris-{4-[2-(4-tert-butyl-phenyl)-vinyl]-3-methyl-phenyl}-methyl)-phenol

Base Information

Chemical Name:4-(tris-{4-[2-(4-tert-butyl-phenyl)-vinyl]-3-methyl-phenyl}-methyl)-phenol
CAS No.:444084-19-9
Molecular Formula:C₆₄H₆₈O
Molecular Weight:853.243
Hs Code.:

4-(tris-{4-[2-(4-<i>tert</i>-butyl-phenyl)-vinyl]-3-methyl-phenyl}-methyl)-phenol

Synonyms:4-(tris-{4-[2-(4-tert-butyl-phenyl)-vinyl]-3-methyl-phenyl}-methyl)-phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(tris-{4-[2-(4-tert-butyl-phenyl)-vinyl]-3-methyl-phenyl}-methyl)-phenol

Chemical Property:

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Technology Process of 4-(tris-{4-[2-(4-tert-butyl-phenyl)-vinyl]-3-methyl-phenyl}-methyl)-phenol

There total 4 articles about 4-(tris-{4-[2-(4-tert-butyl-phenyl)-vinyl]-3-methyl-phenyl}-methyl)-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1746-23-2,26009-55-2
4-tert-Butylstyrene

: 256224-21-2
tris(4'-iodo-3'-methylphenyl)-4-methylphenol

: 444084-19-9
4-(tris-{4-[2-(4-tert-butyl-phenyl)-vinyl]-3-methyl-phenyl}-methyl)-phenol

Guidance literature:: With tetrabutylammomium bromide; potassium acetate; palladium diacetate; In N,N-dimethyl-formamide; at 100 ℃;
DOI:10.1055/s-2003-42119 DOI:10.1016/j.tetlet.2004.02.068

Reference yield:

: 108-95-2,27073-41-2
phenol

: 444084-19-9
4-(tris-{4-[2-(4-tert-butyl-phenyl)-vinyl]-3-methyl-phenyl}-methyl)-phenol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / H₂SO₄ / 80 °C

2: 75 percent / Bu₄NBr; KOAc / Pd(OAc)2 / dimethylformamide / 100 °C

With sulfuric acid; tetrabutylammomium bromide; potassium acetate; palladium diacetate; In N,N-dimethyl-formamide; 2: Heck reaction;
DOI:10.1055/s-2003-42119 DOI:10.1016/j.tetlet.2004.02.068

Reference yield:

: 3248-91-7
New fuchsine

: 444084-19-9
4-(tris-{4-[2-(4-tert-butyl-phenyl)-vinyl]-3-methyl-phenyl}-methyl)-phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaNO₂ / aq. H₂SO₄ / 0 °C

1.2: 40 percent / KI / H₂O / 20 °C

2.1: 85 percent / H₂SO₄ / 80 °C

3.1: 75 percent / Bu₄NBr; KOAc / Pd(OAc)2 / dimethylformamide / 100 °C

With sulfuric acid; tetrabutylammomium bromide; potassium acetate; sodium nitrite; palladium diacetate; In sulfuric acid; N,N-dimethyl-formamide; 3.1: Heck reaction;
DOI:10.1016/j.tetlet.2004.02.068