C₅₁H₆₂N₂O₅Si

Base Information

Chemical Name:C₅₁H₆₂N₂O₅Si
CAS No.:928658-04-2
Molecular Formula:C₅₁H₆₂N₂O₅Si
Molecular Weight:811.149
Hs Code.:

C<sub>51</sub>H<sub>62</sub>N<sub>2</sub>O<sub>5</sub>Si

Synonyms:C₅₁H₆₂N₂O₅Si

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Chemical Property of C₅₁H₆₂N₂O₅Si

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Technology Process of C₅₁H₆₂N₂O₅Si

There total 24 articles about C₅₁H₆₂N₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 928657-94-7
C₅₃H₆₇NO₁₁S₂Si

: 928658-04-2
C₅₁H₆₂N₂O₅Si

Guidance literature:: With ammonia; In tetrahydrofuran; ethanol; at 85 ℃; for 13h;
DOI:10.1021/ja068047t

Reference yield:

: 928657-76-5
C₇H₈Br₂O₂

: 928658-04-2
C₅₁H₆₂N₂O₅Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: 41.76 g / imidazole; N,N-dimethylaminopyridine / dimethylformamide / 14 h / 20 °C

2.1: n-BuLi / diethyl ether; hexane / 0.5 h / -78 °C

2.2: 65 percent / diethyl ether; hexane / 0.5 h / Heating

3.1: 4 Angstroem molecular sieves / Yb(OTf)3*xH₂O / toluene / 3 h / 20 °C

3.2: toluene / 20 h / 100 °C

4.1: 87 percent / DIBAL / CH₂Cl₂; toluene / 0.25 h / -78 °C

5.1: t-BuOK / tetrahydrofuran / 0.17 h / cooling

5.2: 93 percent / tetrahydrofuran / 11 h

6.1: 82 percent / NEt₃; Ag₂SO₄ / Pd(PPh₃)4 / dimethylformamide / 1 h / Heating

7.1: 58 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone; H₂O / CH₂Cl₂ / 5 h / 20 °C

8.1: 89 percent / Et₃N / CH₂Cl₂ / 18 h / 20 °C

9.1: SmI₂ / tetrahydrofuran / 0.5 h / 0 °C

9.2: 1.36 g / aq. NaHCO₃ / tetrahydrofuran / 0.08 h

10.1: 1.34 g / Et₃N; DMAP / CH₂Cl₂ / 0.33 h / 0 °C

11.1: 1.10 g / KOtBu / tetrahydrofuran / 0.58 h / -30 - -20 °C

12.1: 67 percent / NiCl₂*6H₂O; Na₂CO₃; NaBH₄ / tetrahydrofuran; methanol / 2.83 h / -50 °C

13.1: LiAlH₄ / tetrahydrofuran; diethyl ether / 0.25 h / 0 °C

14.1: 1.232 g / Et₃N; DMAP / CH₂Cl₂ / 1 h / 0 °C

15.1: NH₃ / ethanol; tetrahydrofuran / 13 h / 85 °C

With 1H-imidazole; dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; n-butyllithium; samarium diiodide; 4 A molecular sieve; potassium tert-butylate; ammonia; water; diisobutylaluminium hydride; sodium carbonate; silver sulfate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; nickel dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ytterbium(III) triflate; In tetrahydrofuran; methanol; diethyl ether; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; 5.2: Horner-Emmons olefination / 6.1: Heck cyclization;
DOI:10.1021/ja068047t

Reference yield:

: 928657-79-8
C₄₇H₅₄BrNO₉Si

: 928658-04-2
C₅₁H₆₂N₂O₅Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: 87 percent / DIBAL / CH₂Cl₂; toluene / 0.25 h / -78 °C

2.1: t-BuOK / tetrahydrofuran / 0.17 h / cooling

2.2: 93 percent / tetrahydrofuran / 11 h

3.1: 82 percent / NEt₃; Ag₂SO₄ / Pd(PPh₃)4 / dimethylformamide / 1 h / Heating

4.1: 58 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone; H₂O / CH₂Cl₂ / 5 h / 20 °C

5.1: 89 percent / Et₃N / CH₂Cl₂ / 18 h / 20 °C

6.1: SmI₂ / tetrahydrofuran / 0.5 h / 0 °C

6.2: 1.36 g / aq. NaHCO₃ / tetrahydrofuran / 0.08 h

7.1: 1.34 g / Et₃N; DMAP / CH₂Cl₂ / 0.33 h / 0 °C

8.1: 1.10 g / KOtBu / tetrahydrofuran / 0.58 h / -30 - -20 °C

9.1: 67 percent / NiCl₂*6H₂O; Na₂CO₃; NaBH₄ / tetrahydrofuran; methanol / 2.83 h / -50 °C

10.1: LiAlH₄ / tetrahydrofuran; diethyl ether / 0.25 h / 0 °C

11.1: 1.232 g / Et₃N; DMAP / CH₂Cl₂ / 1 h / 0 °C

12.1: NH₃ / ethanol; tetrahydrofuran / 13 h / 85 °C

With dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; samarium diiodide; potassium tert-butylate; ammonia; water; diisobutylaluminium hydride; sodium carbonate; silver sulfate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; nickel dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; 2.2: Horner-Emmons olefination / 3.1: Heck cyclization;
DOI:10.1021/ja068047t