tert-butyl 2,3,4-tri-O-acetyl-6-O-[2,3-di-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-β-D-glucopyranosyl]-β-D-glucopyranoside

Base Information

Chemical Name:tert-butyl 2,3,4-tri-O-acetyl-6-O-[2,3-di-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-β-D-glucopyranosyl]-β-D-glucopyranoside
CAS No.:1022927-43-0
Molecular Formula:C₄₀H₄₆Br₂O₁₈
Molecular Weight:974.602
Hs Code.:

Synonyms:tert-butyl 2,3,4-tri-O-acetyl-6-O-[2,3-di-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-β-D-glucopyranosyl]-β-D-glucopyranoside

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Chemical Property of tert-butyl 2,3,4-tri-O-acetyl-6-O-[2,3-di-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-β-D-glucopyranosyl]-β-D-glucopyranoside

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Technology Process of tert-butyl 2,3,4-tri-O-acetyl-6-O-[2,3-di-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-β-D-glucopyranosyl]-β-D-glucopyranoside

There total 7 articles about tert-butyl 2,3,4-tri-O-acetyl-6-O-[2,3-di-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-β-D-glucopyranosyl]-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1022927-11-2
tert-butyl 2-O-acetyl-6-O-[2-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-β-D-glucopyranosyl]-β-D-glucopyranoside

: 108-24-7
acetic anhydride

: 1022927-43-0
tert-butyl 2,3,4-tri-O-acetyl-6-O-[2,3-di-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-β-D-glucopyranosyl]-β-D-glucopyranoside

Guidance literature:: With pyridine;
DOI:10.1021/jo800191z

Reference yield:

: C₂₆H₄₀O₁₆

: 586-75-4
4-chlorobenzoyl chloride

: 1022927-43-0
tert-butyl 2,3,4-tri-O-acetyl-6-O-[2,3-di-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-β-D-glucopyranosyl]-β-D-glucopyranoside

Guidance literature:: With pyridine; dmap; at 60 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2012.04.035

Reference yield:

: C₃₃H₄₄O₁₆

: 1022927-43-0
tert-butyl 2,3,4-tri-O-acetyl-6-O-[2,3-di-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-β-D-glucopyranosyl]-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / water / 3 h / Reflux; Inert atmosphere

2: pyridine; dmap / 60 °C / Inert atmosphere

With pyridine; dmap; acetic acid; In water;
DOI:10.1016/j.bmcl.2012.04.035