8-methoxycarbonyloctyl 3-O-benzyl-2-deoxy-6-O-(4-methoxybenzyl)-2-phthalimido-4-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:8-methoxycarbonyloctyl 3-O-benzyl-2-deoxy-6-O-(4-methoxybenzyl)-2-phthalimido-4-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-β-D-glucopyranoside
CAS No.:106445-29-8
Molecular Formula:C₅₉H₆₆N₂O₁₉
Molecular Weight:1107.18
Hs Code.:

8-methoxycarbonyloctyl 3-O-benzyl-2-deoxy-6-O-(4-methoxybenzyl)-2-phthalimido-4-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-β-D-glucopyranoside

Synonyms:8-methoxycarbonyloctyl 3-O-benzyl-2-deoxy-6-O-(4-methoxybenzyl)-2-phthalimido-4-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-methoxycarbonyloctyl 3-O-benzyl-2-deoxy-6-O-(4-methoxybenzyl)-2-phthalimido-4-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-β-D-glucopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 8-methoxycarbonyloctyl 3-O-benzyl-2-deoxy-6-O-(4-methoxybenzyl)-2-phthalimido-4-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-β-D-glucopyranoside

There total 8 articles about 8-methoxycarbonyloctyl 3-O-benzyl-2-deoxy-6-O-(4-methoxybenzyl)-2-phthalimido-4-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 106445-28-7
8-methoxycarbonyloctyl 3-O-benzyl-2-deoxy-6-O-(4-methoxybenzyl)-2-phthalimido-β-D-glucopyranoside

: 10028-45-2
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl bromide

: 106445-29-8
8-methoxycarbonyloctyl 3-O-benzyl-2-deoxy-6-O-(4-methoxybenzyl)-2-phthalimido-4-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-β-D-glucopyranoside

Guidance literature:: With 2,3,5-trimethyl-pyridine; silver trifluoromethanesulfonate; In nitromethane; 1) -25 deg C, 30 min, 2) RT, 4.5 h;

Reference yield:

: 3639-34-7
8-ethoxycarbonyloctanol

: 106445-29-8
8-methoxycarbonyloctyl 3-O-benzyl-2-deoxy-6-O-(4-methoxybenzyl)-2-phthalimido-4-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 54 percent / silver zeolite / CH₂Cl₂ / 40 h / Ambient temperature

2: 99 percent / methanol / 0.5 h

3: 64 percent / p-TsOH*H₂O / acetonitrile / 0.83 h / Ambient temperature

4: 90 percent / 1) NaH / tetrahydrofuran / 21 h / Ambient temperature

5: 1) sodium cyanoborohydride, mol. sieves 3A, 2) TFA / 1) DMF, 15 min, RT, 2) DMF, 43 h

6: 66 percent / silver triflate, collidine / nitromethane / 1) -25 deg C, 30 min, 2) RT, 4.5 h

With 2,3,5-trimethyl-pyridine; 3 A molecular sieve; silver zeolite; silver trifluoromethanesulfonate; sodium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; methanol; nitromethane; dichloromethane; acetonitrile;

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 106445-29-8
8-methoxycarbonyloctyl 3-O-benzyl-2-deoxy-6-O-(4-methoxybenzyl)-2-phthalimido-4-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / p-TsOH*H₂O / acetonitrile / 0.83 h / Ambient temperature

2: 90 percent / 1) NaH / tetrahydrofuran / 21 h / Ambient temperature

3: 1) sodium cyanoborohydride, mol. sieves 3A, 2) TFA / 1) DMF, 15 min, RT, 2) DMF, 43 h

4: 66 percent / silver triflate, collidine / nitromethane / 1) -25 deg C, 30 min, 2) RT, 4.5 h

With 2,3,5-trimethyl-pyridine; 3 A molecular sieve; silver trifluoromethanesulfonate; sodium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; nitromethane; acetonitrile;