15-Hydroxy-19-methyl-17-oxapentacyclo[6.6.5.02,7.09,14.015,19]nonadeca-2,4,6,9,11,13-hexaene-16,18-dione

Base Information

• Chemical Name: 15-Hydroxy-19-methyl-17-oxapentacyclo[6.6.5.02,7.09,14.015,19]nonadeca-2,4,6,9,11,13-hexaene-16,18-dione
• CAS No.: 5469-62-5
• Molecular Formula: C₁₉H₁₄O₄
• Molecular Weight: 306.318
• NSC Number: 25355

Synonyms:NSC25355;5469-62-5;NSC-25355

Chemical Property of 15-Hydroxy-19-methyl-17-oxapentacyclo[6.6.5.02,7.09,14.015,19]nonadeca-2,4,6,9,11,13-hexaene-16,18-dione

Chemical Property:

• Vapor Pressure: 7.45E-12mmHg at 25°C
• XLogP3: 2.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 306.08920892
• Heavy Atom Count: 23
• Complexity: 562

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC12C3C4=CC=CC=C4C(C1(C(=O)OC2=O)O)C5=CC=CC=C35

Technology Process of 15-Hydroxy-19-methyl-17-oxapentacyclo[6.6.5.02,7.09,14.015,19]nonadeca-2,4,6,9,11,13-hexaene-16,18-dione

There total 1 articles about 15-Hydroxy-19-methyl-17-oxapentacyclo[6.6.5.02,7.09,14.015,19]nonadeca-2,4,6,9,11,13-hexaene-16,18-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 11-hydroxy-12-methyl-9,10-dihydro-9,10-ethano-anthracene-11,12-dicarboxylic acid-anhydride (5469-62-5)

Guidance literature:

With sodium hydroxide; Behandeln des Reaktionsprodukts mit wss. Salzsaeure;

DOI:10.1021/ja01142a026

Reference yield:

hydrogen bromide (10035-10-6,12258-64-9) + 11-hydroxy-12-methyl-9,10-dihydro-9,10-ethano-anthracene-11,12-dicarboxylic acid-anhydride (5469-62-5) → anthracene (120-12-7) + 12-methyl-9,10-dihydro-9,10-ethano-anthracen-11-one (53482-99-8)

Guidance literature:

at 175 ℃;

DOI:10.1021/ja01142a026

Downstream raw materials:

anthracene

12-methyl-9,10-dihydro-9,10-ethano-anthracen-11-one

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