N-mesyl-6-methoxy-2-(4,5,6-trimethoxy-2-methoxycarbonylanilino)-p-benzoquinone

Base Information

Chemical Name:N-mesyl-6-methoxy-2-(4,5,6-trimethoxy-2-methoxycarbonylanilino)-p-benzoquinone
CAS No.:153779-33-0
Molecular Formula:C₁₉H₂₁NO₁₀S
Molecular Weight:455.442
Hs Code.:

Synonyms:N-mesyl-6-methoxy-2-(4,5,6-trimethoxy-2-methoxycarbonylanilino)-p-benzoquinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-mesyl-6-methoxy-2-(4,5,6-trimethoxy-2-methoxycarbonylanilino)-p-benzoquinone

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Technology Process of N-mesyl-6-methoxy-2-(4,5,6-trimethoxy-2-methoxycarbonylanilino)-p-benzoquinone

There total 1 articles about N-mesyl-6-methoxy-2-(4,5,6-trimethoxy-2-methoxycarbonylanilino)-p-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 54490-80-1
2-chloro-6-methoxy-p-benzoquinone

: 2-Methanesulfonylamino-3,4,5-trimethoxy-benzoic acid methyl ester

: 153779-33-0
N-mesyl-6-methoxy-2-(4,5,6-trimethoxy-2-methoxycarbonylanilino)-p-benzoquinone

Guidance literature:: With 18-crown-6 ether; Celite; cesium fluoride; In N,N-dimethyl-formamide; at 65 ℃; for 4h;

Reference yield:

: 153779-33-0
N-mesyl-6-methoxy-2-(4,5,6-trimethoxy-2-methoxycarbonylanilino)-p-benzoquinone

: 153779-50-1
2-[Methanesulfonyl-(2,3,5-trimethoxy-phenyl)-amino]-3,4,5-trimethoxy-benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) cetyltrimethylammonium bromide, aq. Na₂S₂O₄, 2.) aq. KOH / 1.) THF, 2.) THF, RT, 14 h

2: 87 percent / 2N aq. KOH / 24 h / Ambient temperature

With potassium hydroxide; sodium dithionite; cetyltrimethylammonim bromide;

Reference yield:

: 77-78-1
dimethyl sulfate

: 153779-33-0
N-mesyl-6-methoxy-2-(4,5,6-trimethoxy-2-methoxycarbonylanilino)-p-benzoquinone

: 153779-49-8
N-mesyl-1,4,6-trimethoxy-2-(4,5,6-trimethoxy-2-methoxycarbonylanilino)benzene

Guidance literature:: With potassium hydroxide; sodium dithionite; cetyltrimethylammonim bromide; Yield given. Multistep reaction; 1.) THF, 2.) THF, RT, 14 h;