N-(4-(trifluoromethyl)-2-(1H-pyrazol-1-yl)phenyl)-4-methyl-2-(1H-pyrazol-1-yl)benzenamine

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Chemical Name:N-(4-(trifluoromethyl)-2-(1H-pyrazol-1-yl)phenyl)-4-methyl-2-(1H-pyrazol-1-yl)benzenamine
CAS No.:1345047-54-2
Molecular Formula:C₂₀H₁₆F₃N₅
Molecular Weight:383.376
Hs Code.:

Synonyms:N-(4-(trifluoromethyl)-2-(1H-pyrazol-1-yl)phenyl)-4-methyl-2-(1H-pyrazol-1-yl)benzenamine

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Chemical Property of N-(4-(trifluoromethyl)-2-(1H-pyrazol-1-yl)phenyl)-4-methyl-2-(1H-pyrazol-1-yl)benzenamine

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Technology Process of N-(4-(trifluoromethyl)-2-(1H-pyrazol-1-yl)phenyl)-4-methyl-2-(1H-pyrazol-1-yl)benzenamine

There total 5 articles about N-(4-(trifluoromethyl)-2-(1H-pyrazol-1-yl)phenyl)-4-methyl-2-(1H-pyrazol-1-yl)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: N-(2-amino-5-methylphenyl)-1H-pyrazole

: 1345047-52-0
1-(2-bromo-5-trifluoromethylphenyl)-1H-pyrazole

: 1345047-54-2
N-(4-(trifluoromethyl)-2-(1H-pyrazol-1-yl)phenyl)-4-methyl-2-(1H-pyrazol-1-yl)benzenamine

Guidance literature:: With copper(l) iodide; caesium carbonate; In 1,4-dioxane; for 15h; Inert atmosphere; Reflux;
DOI:10.1016/j.jorganchem.2011.08.013

Reference yield:

2-bromo-p-toluidine: 583-68-6
2-bromo-p-toluidine

: 1345047-54-2
N-(4-(trifluoromethyl)-2-(1H-pyrazol-1-yl)phenyl)-4-methyl-2-(1H-pyrazol-1-yl)benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; caesium carbonate / N,N-dimethyl-formamide

2: copper(l) iodide; caesium carbonate / 1,4-dioxane / 15 h / Inert atmosphere; Reflux

With copper(l) iodide; caesium carbonate; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.jorganchem.2011.08.013

Reference yield:

: 40161-54-4
1-bromo-2-fluoro-4-(trifluoromethyl)benzene

: 1345047-54-2
N-(4-(trifluoromethyl)-2-(1H-pyrazol-1-yl)phenyl)-4-methyl-2-(1H-pyrazol-1-yl)benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h

1.2: 0.5 h / Reflux

2.1: copper(l) iodide; caesium carbonate / 1,4-dioxane / 15 h / Inert atmosphere; Reflux

With copper(l) iodide; sodium hydride; caesium carbonate; In 1,4-dioxane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.jorganchem.2011.08.013