[N-(3-((tert-butyldimethylsilyl)oxy)allyl)-3-methoxy-N-phenylcyclohexa-1,3-dienecarboxamide]tricarbonyliron

Base Information

• Chemical Name: [N-(3-((tert-butyldimethylsilyl)oxy)allyl)-3-methoxy-N-phenylcyclohexa-1,3-dienecarboxamide]tricarbonyliron
• CAS No.: 1400786-12-0
• Molecular Formula: C₂₆H₃₃FeNO₆Si
• Molecular Weight: 539.484

Synonyms:[N-(3-((tert-butyldimethylsilyl)oxy)allyl)-3-methoxy-N-phenylcyclohexa-1,3-dienecarboxamide]tricarbonyliron

Chemical Property of [N-(3-((tert-butyldimethylsilyl)oxy)allyl)-3-methoxy-N-phenylcyclohexa-1,3-dienecarboxamide]tricarbonyliron

Chemical Property:

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Technology Process of [N-(3-((tert-butyldimethylsilyl)oxy)allyl)-3-methoxy-N-phenylcyclohexa-1,3-dienecarboxamide]tricarbonyliron

There total 2 articles about [N-(3-((tert-butyldimethylsilyl)oxy)allyl)-3-methoxy-N-phenylcyclohexa-1,3-dienecarboxamide]tricarbonyliron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyldimethylsilyl 2-methylpropane-2-sulfonate (1027156-11-1) + [3-methoxy-N-(3-oxopropyl)-N-phenylcyclohexa-1,3-dienecarboxamide]tricarbonyl iron (1400786-10-8) → [N-(3-((tert-butyldimethylsilyl)oxy)allyl)-3-methoxy-N-phenylcyclohexa-1,3-dienecarboxamide]tricarbonyl iron (1400786-12-0) + [N-(3-((tert-butyldimethylsilyl)oxy)allyl)-3-methoxy-N-phenylcyclohexa-1,3-dienecarboxamide]tricarbonyl iron (1400786-12-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 2h; Overall yield = 80 %; Overall yield = 39.3 mg; Inert atmosphere;

DOI:10.1021/jo301721d

Reference yield:

tert-butyldimethylsilyl 2-methylpropane-2-sulfonate (1027156-11-1) + [3-methoxy-N-(3-oxopropyl)-N-phenylcyclohexa-1,3-dienecarboxamide]tricarbonyl iron (1400786-10-8) → [N-(3-((tert-butyldimethylsilyl)oxy)allyl)-3-methoxy-N-phenylcyclohexa-1,3-dienecarboxamide]tricarbonyl iron (1400786-12-0) + [N-(3-((tert-butyldimethylsilyl)oxy)allyl)-3-methoxy-N-phenylcyclohexa-1,3-dienecarboxamide]tricarbonyl iron (1400786-12-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 2h; Overall yield = 80 %; Overall yield = 39.3 mg; Inert atmosphere;

DOI:10.1021/jo301721d

Reference yield: 35.0%

[N-(3-((tert-butyldimethylsilyl)oxy)allyl)-3-methoxy-N-phenylcyclohexa-1,3-dienecarboxamide]tricarbonyliron (1400786-12-0) → [4-(((tert-butyldimethylsilyl)oxy)methyl)-9-methoxy-2-phenyl-2-azaspiro[4.5]deca-6,8-dien-1-one]tricarbonyl iron + [4-(((tert-butyldimethylsilyl)oxy)methyl)-7-methoxy-2-phenyl-2-azaspiro[4.5]deca-6,8-dien-1-one]tricarbonyl iron

Guidance literature:

With carbon monoxide; In dibutyl ether; at 142 ℃; for 20h; Inert atmosphere;

DOI:10.1021/jo301721d

upstream raw materials:

tert-butyldimethylsilyl 2-methylpropane-2-sulfonate

[3-methoxy-N-(3-oxopropyl)-N-phenylcyclohexa-1,3-dienecarboxamide]tricarbonyl iron

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