(+/-)-3-<(4-tert-Butylphenyl)-amino>tetrahydro-4-(hydroxymethyl)-2-methylfuran

Base Information

Chemical Name:(+/-)-3-<(4-tert-Butylphenyl)-amino>tetrahydro-4-(hydroxymethyl)-2-methylfuran
CAS No.:134236-98-9
Molecular Formula:C₁₆H₂₅NO₂
Molecular Weight:263.38
Hs Code.:

Synonyms:(+/-)-3-<(4-tert-Butylphenyl)-amino>tetrahydro-4-(hydroxymethyl)-2-methylfuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-3-<(4-tert-Butylphenyl)-amino>tetrahydro-4-(hydroxymethyl)-2-methylfuran

Chemical Property:

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Technology Process of (+/-)-3-<(4-tert-Butylphenyl)-amino>tetrahydro-4-(hydroxymethyl)-2-methylfuran

There total 4 articles about (+/-)-3-<(4-tert-Butylphenyl)-amino>tetrahydro-4-(hydroxymethyl)-2-methylfuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 134236-89-8
(+/-)-2-(4-tert-Butylphenyl)-8-methyl-3,7-dioxa-2-azabicyclo<3.3,0>octan

: 134236-98-9
(+/-)-3-<(4-tert-Butylphenyl)-amino>tetrahydro-4-(hydroxymethyl)-2-methylfuran

Guidance literature:: nickel; In isopropyl alcohol; Ambient temperature;

Reference yield:

: 13252-73-8
N-(4-tert-Butylphenyl)hydroxylamine

: 134236-98-9
(+/-)-3-<(4-tert-Butylphenyl)-amino>tetrahydro-4-(hydroxymethyl)-2-methylfuran

Guidance literature:: Multi-step reaction with 2 steps

1: MgSO₄ / diethyl ether / 1a) 0 deg C, 2 h, b) r. t., 18 h

2: 95 percent / active Raney-nickel / propan-2-ol / Ambient temperature

With magnesium sulfate; nickel; In diethyl ether; isopropyl alcohol;

Reference yield:

: 114209-13-1
rac-2-Methyl-3-oxa-5-hexensaeure-methylester

: 134236-98-9
(+/-)-3-<(4-tert-Butylphenyl)-amino>tetrahydro-4-(hydroxymethyl)-2-methylfuran

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminum hydride / diethyl ether; hexane / 1 h / -78 °C

2: MgSO₄ / diethyl ether / 1a) 0 deg C, 2 h, b) r. t., 18 h

3: 95 percent / active Raney-nickel / propan-2-ol / Ambient temperature

With diisobutylaluminium hydride; magnesium sulfate; nickel; In diethyl ether; hexane; isopropyl alcohol;