phosphoric acid dibenzyl ester 1-(2-dimethylamino-ethylcarbamoyl)-5,6-dimethyl-6H-pyrido[4,3-b]carbazol-9-yl ester

Base Information

• Chemical Name: phosphoric acid dibenzyl ester 1-(2-dimethylamino-ethylcarbamoyl)-5,6-dimethyl-6H-pyrido[4,3-b]carbazol-9-yl ester
• CAS No.: 231297-45-3
• Molecular Formula: C₃₆H₃₇N₄O₅P
• Molecular Weight: 636.687

Synonyms:phosphoric acid dibenzyl ester 1-(2-dimethylamino-ethylcarbamoyl)-5,6-dimethyl-6H-pyrido[4,3-b]carbazol-9-yl ester

Chemical Property of phosphoric acid dibenzyl ester 1-(2-dimethylamino-ethylcarbamoyl)-5,6-dimethyl-6H-pyrido[4,3-b]carbazol-9-yl ester

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Technology Process of phosphoric acid dibenzyl ester 1-(2-dimethylamino-ethylcarbamoyl)-5,6-dimethyl-6H-pyrido[4,3-b]carbazol-9-yl ester

There total 1 articles about phosphoric acid dibenzyl ester 1-(2-dimethylamino-ethylcarbamoyl)-5,6-dimethyl-6H-pyrido[4,3-b]carbazol-9-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate (990-91-0) + N-[2-(dimethylamino)ethyl]-9-hydroxy-5,6-dimethyl-6H-pyrido[4,3-b]carbazole-1-carboxamide (156055-46-8) → phosphoric acid dibenzyl ester 1-(2-dimethylamino-ethylcarbamoyl)-5,6-dimethyl-6H-pyrido[4,3-b]carbazol-9-yl ester (231297-45-3)

Guidance literature:

With sodium hydride; Yield given; Multistep reaction; 1.) THF, RT, 1 h, 2.) THF, RT, 6 h;

DOI:10.1021/jm981093m

Reference yield: 62.8%

phosphoric acid dibenzyl ester 1-(2-dimethylamino-ethylcarbamoyl)-5,6-dimethyl-6H-pyrido[4,3-b]carbazol-9-yl ester (231297-45-3) → benzyl<2-(5,6-dimethyl-9-(benzylphosphate)-6H-pyrido<4,3-b>carbazol-1-yl)carbonylaminoethyl>methylammonium

Guidance literature:

for 96h; Ambient temperature;

DOI:10.1021/jm981093m

Reference yield: 43.5%

phosphoric acid dibenzyl ester 1-(2-dimethylamino-ethylcarbamoyl)-5,6-dimethyl-6H-pyrido[4,3-b]carbazol-9-yl ester (231297-45-3) → phosphoric acid benzyl ester 1-(2-dimethylamino-ethylcarbamoyl)-5,6-dimethyl-6H-pyrido[4,3-b]carbazol-9-yl ester

Guidance literature:

With cyclohexene; palladium on activated charcoal; In various solvent(s); at 100 ℃; for 0.583333h;

DOI:10.1021/jm981093m

upstream raw materials:

dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate

N-[2-(dimethylamino)ethyl]-9-hydroxy-5,6-dimethyl-6H-pyrido[4,3-b]carbazole-1-carboxamide

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