Technology Process of C19H24N4O5S
There total 9 articles about C19H24N4O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrazine hydrate;
In
ethanol;
at 20 - 70 ℃;
for 15h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: water / tetrahydrofuran / 2.5 h / Reflux
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 5 h / 20 °C
3: hydrogenchloride / 1,4-dioxane / 20 °C
4: sodium hydrogencarbonate / water; tetrahydrofuran
5: hydrazine hydrate / ethanol / 15 h / 20 - 70 °C
With
hydrogenchloride; water; sodium hydrogencarbonate; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium azide / N,N-dimethyl-formamide / 23 h / 50 °C
2: water / tetrahydrofuran / 2.5 h / Reflux
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 5 h / 20 °C
4: hydrogenchloride / 1,4-dioxane / 20 °C
5: sodium hydrogencarbonate / water; tetrahydrofuran
6: hydrazine hydrate / ethanol / 15 h / 20 - 70 °C
With
hydrogenchloride; sodium azide; water; sodium hydrogencarbonate; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
