N-<1-(carbazoylmethyl)-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide

Base Information

Chemical Name:N-<1-(carbazoylmethyl)-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide
CAS No.:161038-46-6
Molecular Formula:C₁₈H₁₉N₅O₄
Molecular Weight:369.38
Hs Code.:

Synonyms:N-<1-(carbazoylmethyl)-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<1-(carbazoylmethyl)-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide

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Technology Process of N-<1-(carbazoylmethyl)-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide

There total 1 articles about N-<1-(carbazoylmethyl)-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 161038-45-5
methyl 3-(benzoylamino)-2,5,6,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepine-1-acetate

: 161038-46-6
N-<1-(carbazoylmethyl)-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide

Guidance literature:: With hydrazine hydrate; In ethanol; for 4h; Heating;
DOI:10.1002/jhet.5570310601

Reference yield: 86.0%

: 161038-46-6
N-<1-(carbazoylmethyl)-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide

: 161038-47-7
N-<1-<(azidocarbonyl)methyl>-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide

Guidance literature:: With hydrogenchloride; sodium nitrite; at 0 ℃; for 5h;
DOI:10.1002/jhet.5570310601

Reference yield:

: 161038-46-6
N-<1-(carbazoylmethyl)-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide

: 161038-50-2
N-<2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / 36percent aq. HCl, NaNO₂ / 5 h / 0 °C

2: 100 percent / 4 h / 110 °C

3: 5percent aq. KOH / 0.5 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; sodium nitrite;
DOI:10.1002/jhet.5570310601