[palladium(bromide)(1,2-bis(diphenylphosphine)ethane)(CH₂C₆H₂(t-Bu)2OSiMe₃)]

Base Information

• Chemical Name: [palladium(bromide)(1,2-bis(diphenylphosphine)ethane)(CH₂C₆H₂(t-Bu)2OSiMe₃)]
• CAS No.: 211241-09-7
• Molecular Formula: C₄₄H₅₅BrOP₂PdSi
• Molecular Weight: 876.277

Synonyms:[palladium(bromide)(1,2-bis(diphenylphosphine)ethane)(CH₂C₆H₂(t-Bu)2OSiMe₃)]

Chemical Property of [palladium(bromide)(1,2-bis(diphenylphosphine)ethane)(CH₂C₆H₂(t-Bu)2OSiMe₃)]

Chemical Property:

Purity/Quality:

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Technology Process of [palladium(bromide)(1,2-bis(diphenylphosphine)ethane)(CH₂C₆H₂(t-Bu)2OSiMe₃)]

There total 2 articles about [palladium(bromide)(1,2-bis(diphenylphosphine)ethane)(CH₂C₆H₂(t-Bu)2OSiMe₃)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[4-(Bromomethyl)-2,6-di-tert-butylphenoxy]trimethylsilylane (211241-07-5) → [palladium(bromide)(1,2-bis(diphenylphosphine)ethane)(CH2C6H2(t-Bu)2OSiMe3)] (211241-09-7)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone

In acetone;

DOI:10.1021/ja9809612

Reference yield:

[palladium(bromide)(tetramethylethylenediamine)(CH2C6H2(t-Bu)2OSiMe3)] (211241-08-6) + 1,2-bis-(diphenylphosphino)ethane (1663-45-2) → [palladium(bromide)(1,2-bis(diphenylphosphine)ethane)(CH2C6H2(t-Bu)2OSiMe3)] (211241-09-7)

Guidance literature:

DOI:10.1021/ja9809612

Reference yield: 91.0%

[palladium(bromide)(1,2-bis(diphenylphosphine)ethane)(CH2C6H2(t-Bu)2OSiMe3)] (211241-09-7) → [palladium(1,2-bis(diphenylphosphine)ethane)(η2-CH2C6H2(t-Bu)2)O] (211241-10-0)

Guidance literature:

With (n-Bu)4NF*3H₂O; In tetrahydrofuran;

DOI:10.1021/ja9809612

upstream raw materials:

[palladium(bromide)(tetramethylethylenediamine)(CH₂C₆H₂(t-Bu)2OSiMe₃)]

1,2-bis-(diphenylphosphino)ethane

[4-(Bromomethyl)-2,6-di-tert-butylphenoxy]trimethylsilylane

Downstream raw materials:

[palladium(1,2-bis(diphenylphosphine)ethane)(η²-CH2C6H2(t-Bu)2)O]

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