3,3'-bis{[1,4,7-tri(trifluoroacetyl)-1,4,7,10-tetraazacyclododecan-1-yl]-methyl}-1,1',1''-triphenylmethane

Base Information

Chemical Name:3,3'-bis{[1,4,7-tri(trifluoroacetyl)-1,4,7,10-tetraazacyclododecan-1-yl]-methyl}-1,1',1''-triphenylmethane
CAS No.:1093678-51-3
Molecular Formula:C₄₉H₅₀F₁₈N₈O₆
Molecular Weight:1188.96
Hs Code.:

Synonyms:3,3'-bis{[1,4,7-tri(trifluoroacetyl)-1,4,7,10-tetraazacyclododecan-1-yl]-methyl}-1,1',1''-triphenylmethane

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Chemical Property of 3,3'-bis{[1,4,7-tri(trifluoroacetyl)-1,4,7,10-tetraazacyclododecan-1-yl]-methyl}-1,1',1''-triphenylmethane

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Technology Process of 3,3'-bis{[1,4,7-tri(trifluoroacetyl)-1,4,7,10-tetraazacyclododecan-1-yl]-methyl}-1,1',1''-triphenylmethane

There total 1 articles about 3,3'-bis{[1,4,7-tri(trifluoroacetyl)-1,4,7,10-tetraazacyclododecan-1-yl]-methyl}-1,1',1''-triphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1093678-35-3
3,3'-(phenyl)methylenedibenzyl bromide

: 1,4,7-tris-(trifluoroacetyl)-1,4,7,10-tetraazacyclododecane

: 1093678-51-3
3,3'-bis{[1,4,7-tri(trifluoroacetyl)-1,4,7,10-tetraazacyclododecan-1-yl]-methyl}-1,1',1''-triphenylmethane

Guidance literature:: With potassium carbonate; In acetonitrile; for 24h; Reflux;

Reference yield: 55.0%

: 1093678-51-3
3,3'-bis{[1,4,7-tri(trifluoroacetyl)-1,4,7,10-tetraazacyclododecan-1-yl]-methyl}-1,1',1''-triphenylmethane

: 3,3'-bis[(1,4,7,10-tetraazacyclododecan-1-yl)-methyl]-1,1',1''-triphenylmethane octahydrochloride

Guidance literature:: 3,3'-bis{[1,4,7-tri(trifluoroacetyl)-1,4,7,10-tetraazacyclododecan-1-yl]-methyl}-1,1',1''-triphenylmethane; With potassium carbonate; In methanol; Reflux;

With hydrogenchloride; In methanol; diethyl ether; for 0.5h;