Technology Process of C12H15N
There total 3 articles about C12H15N which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium fluoride dihydrate;
In
methanol;
at 20 ℃;
for 3h;
DOI:10.1021/ol5002347
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diisopropylamine / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
2: potassium fluoride dihydrate / methanol / 3 h / 20 °C
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium fluoride dihydrate; diisopropylamine;
In
tetrahydrofuran; methanol;
1: |Sonogashira Cross-Coupling;
DOI:10.1021/ol5002347
- Guidance literature:
-
Multi-step reaction with 3 steps
1: boron trifluoride diethyl etherate / hexane / 20 °C / Inert atmosphere
2: diisopropylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
3: potassium fluoride dihydrate / methanol / 12 h / 20 °C
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium fluoride dihydrate; boron trifluoride diethyl etherate; diisopropylamine;
In
tetrahydrofuran; methanol; hexane;
DOI:10.1002/anie.201908961