Cyclohexanamine, 4-(2-methoxyethoxy)-, trans- (9CI)

Base Information

• Chemical Name: Cyclohexanamine, 4-(2-methoxyethoxy)-, trans- (9CI)
• CAS No.: 175867-01-3
• Molecular Formula: C₉H₁₉NO₂
• Molecular Weight: 173.255
• Mol file: 175867-01-3.mol

Synonyms:trans-4-[[2-(Methyloxy)ethyl]oxy]cyclohexanamine

Chemical Property of Cyclohexanamine, 4-(2-methoxyethoxy)-, trans- (9CI)

Chemical Property:

• Boiling Point: 241.0±30.0 °C(Predicted)
• PKA: 10.37±0.70(Predicted)
• PSA: 0.00000
• Density: 0.98±0.1 g/cm3(Predicted)
• LogP: 0.00000
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

97% ^*data from raw suppliers

trans-4-(2-Methoxyethoxy)cyclohexanamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Cyclohexanamine, 4-(2-methoxyethoxy)-, trans- (9CI)

There total 12 articles about Cyclohexanamine, 4-(2-methoxyethoxy)-, trans- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

dibenzyl-[trans-4-(2-methoxy-ethoxy)-cyclohexyl]-amine → trans-4-{[2-(methyloxy)ethyl]oxy}cyclohexanamine (175867-00-2,175867-01-3)

Guidance literature:

With hydrogen; palladium hydroxide on carbon; In ethanol; for 4h; under 2068.65 Torr;

Reference yield: 92.0%

(1r,4r)-N,N-dibenzyl-4-(2-methoxyethoxy)cyclohexan-1-amine → (1r,4r)-4-(2-methoxyethoxy)cyclohexan-1-amine (175867-00-2,175867-01-3)

Guidance literature:

With 10 wt% Pd(OH)2 on carbon; hydrogen; In ethanol; at 20 ℃; for 14h;

Reference yield: 87.0%

trans-N,N-dibenzyl-4-(2-methoxyethoxy)cyclohexanamine hydrochloride salt → (1r,4r)-4-(2-methoxyethoxy)cyclohexan-1-amine (175867-00-2,175867-01-3)

Guidance literature:

trans-N,N-dibenzyl-4-(2-methoxyethoxy)cyclohexanamine hydrochloride salt; With sodium hydroxide; In tert-butyl methyl ether; water; for 0.0833333h;

With 10 wt% Pd(OH)2 on carbon; hydrogen; In ethanol; at 20 ℃; for 4.33h;

upstream raw materials:

trans-4-aminocyclohexan-1-ol

trans-4-hydroxycyclohexylamine

trans-4-(dibenzylamino)cyclohexanol

trans-4-aminocyclohexanol hydrochloride

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