C₂₅H₃₃FN₄O₃

Base Information

Chemical Name:C₂₅H₃₃FN₄O₃
CAS No.:1393746-72-9
Molecular Formula:C₂₅H₃₃FN₄O₃
Molecular Weight:456.56
Hs Code.:

C<sub>25</sub>H<sub>33</sub>FN<sub>4</sub>O<sub>3</sub>

Synonyms:C₂₅H₃₃FN₄O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₃₃FN₄O₃

Chemical Property:

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Technology Process of C₂₅H₃₃FN₄O₃

There total 6 articles about C₂₅H₃₃FN₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₀H₄₁FN₄O₅

: 1393746-72-9
C₂₅H₃₃FN₄O₃

Guidance literature:: With chloro-trimethyl-silane; sodium iodide; In acetonitrile; at 20 ℃; for 2h;
DOI:10.1016/j.bmcl.2012.06.022

Reference yield:

: 72752-81-9
methyl 2-mercapto-1,3-benzoxazole-6-carboxylate

: 1393746-72-9
C₂₅H₃₃FN₄O₃

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / ethyl acetate / 12 h / 20 °C

2: tetrahydrofuran / 70 °C

3: water; lithium hydroxide / tetrahydrofuran / 70 °C

4: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 20 °C

5: chloro-trimethyl-silane; sodium iodide / acetonitrile / 2 h / 20 °C

With chloro-trimethyl-silane; water; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; sodium iodide; lithium hydroxide; In tetrahydrofuran; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/j.bmcl.2012.06.022

Reference yield:

: 1160490-12-9
C₁₂H₁₄N₂O₃

: 1393746-72-9
C₂₅H₃₃FN₄O₃

Guidance literature:: Multi-step reaction with 3 steps

1: water; lithium hydroxide / tetrahydrofuran / 70 °C

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 20 °C

3: chloro-trimethyl-silane; sodium iodide / acetonitrile / 2 h / 20 °C

With chloro-trimethyl-silane; water; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; sodium iodide; lithium hydroxide; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2012.06.022