Technology Process of C13H13Cl2NO
There total 3 articles about C13H13Cl2NO which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride;
In
toluene;
at 40 ℃;
for 1.5h;
Inert atmosphere;
DOI:10.1021/ml300262e
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium hydroxide; water / methanol / 20 - 30 °C
2: triethylamine; 2-chloro-1-methyl-pyridinium iodide / dichloromethane / 1.5 h / 20 °C
3: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 1.5 h / 40 °C / Inert atmosphere
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2-chloro-1-methyl-pyridinium iodide; water; triethylamine; lithium hydroxide;
In
methanol; dichloromethane; toluene;
DOI:10.1021/ml300262e
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine; 2-chloro-1-methyl-pyridinium iodide / dichloromethane / 1.5 h / 20 °C
2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 1.5 h / 40 °C / Inert atmosphere
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2-chloro-1-methyl-pyridinium iodide; triethylamine;
In
dichloromethane; toluene;
DOI:10.1021/ml300262e
