C₃₂H₄₄N₂O₅Si

Base Information

Chemical Name:C₃₂H₄₄N₂O₅Si
CAS No.:1269788-54-6
Molecular Formula:C₃₂H₄₄N₂O₅Si
Molecular Weight:564.797
Hs Code.:

C<sub>32</sub>H<sub>44</sub>N<sub>2</sub>O<sub>5</sub>Si

Synonyms:C₃₂H₄₄N₂O₅Si

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Chemical Property of C₃₂H₄₄N₂O₅Si

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Technology Process of C₃₂H₄₄N₂O₅Si

There total 4 articles about C₃₂H₄₄N₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1269788-53-5
C₃₂H₄₂N₂O₃Si

: 1269788-54-6
C₃₂H₄₄N₂O₅Si

Guidance literature:: With methanesulfonamide; 1,4-bis(9-O-dihydroquinidine)phthalazine; In water; tert-butyl alcohol; at 4 ℃; for 48h; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.12.066

Reference yield:

: 1269788-48-8
benzyl (R,Z)-3-((tert-butyldimethylsilyloxy)methyl)-4-(2-ethoxy-2-oxoethylidene)piperidine-1-carboxylate

: 1269788-54-6
C₃₂H₄₄N₂O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 6 h / 20 °C / Inert atmosphere

2.1: pyridine; dmap / 0.75 h / 0 - 20 °C / Inert atmosphere

3.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

3.2: 12 h / -65 °C / Inert atmosphere

4.1: sodium tetrahydroborate / methanol / 2 h / 20 °C / Cooling with ice; Inert atmosphere

5.1: pyridine / 1.5 h / 0 - 20 °C / Inert atmosphere

6.1: potassium tert-butylate / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

7.1: methanesulfonamide; 1,4-bis(9-O-dihydroquinidine)phthalazine / water; tert-butyl alcohol / 48 h / 4 °C / Inert atmosphere

With pyridine; dmap; sodium tetrahydroborate; n-butyllithium; methanesulfonamide; 20 % Pd(OH)2/C; potassium tert-butylate; hydrogen; 1,4-bis(9-O-dihydroquinidine)phthalazine; diisopropylamine; In tetrahydrofuran; methanol; hexane; water; ethyl acetate; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2010.12.066

Reference yield:

: C₃₃H₄₆N₂O₆SSi

: 1269788-54-6
C₃₂H₄₄N₂O₅Si

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

2: methanesulfonamide; 1,4-bis(9-O-dihydroquinidine)phthalazine / water; tert-butyl alcohol / 48 h / 4 °C / Inert atmosphere

With methanesulfonamide; potassium tert-butylate; 1,4-bis(9-O-dihydroquinidine)phthalazine; In tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2010.12.066