(E)-1-(4'-O-methoxymethylphenyl)-3-(2'',4''-di-O-methoxymethylphenyl)-propene

Base Information

Chemical Name:(E)-1-(4'-O-methoxymethylphenyl)-3-(2'',4''-di-O-methoxymethylphenyl)-propene
CAS No.:251909-44-1
Molecular Formula:C₂₁H₂₆O₆
Molecular Weight:374.434
Hs Code.:

Synonyms:(E)-1-(4'-O-methoxymethylphenyl)-3-(2'',4''-di-O-methoxymethylphenyl)-propene

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Chemical Property of (E)-1-(4'-O-methoxymethylphenyl)-3-(2'',4''-di-O-methoxymethylphenyl)-propene

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Technology Process of (E)-1-(4'-O-methoxymethylphenyl)-3-(2'',4''-di-O-methoxymethylphenyl)-propene

There total 5 articles about (E)-1-(4'-O-methoxymethylphenyl)-3-(2'',4''-di-O-methoxymethylphenyl)-propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 251909-39-4
1-(4'-O-methoxymethylphenyl)-3-(2'',4''-di-O-methoxymethylphenyl)-1-propanol

: 251909-44-1
(E)-1-(4'-O-methoxymethylphenyl)-3-(2'',4''-di-O-methoxymethylphenyl)-propene

Guidance literature:: 1-(4'-O-methoxymethylphenyl)-3-(2'',4''-di-O-methoxymethylphenyl)-1-propanol; With thionyl chloride; In dichloromethane; at 20 ℃; for 0.0833333h;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene; for 12h; Heating;
DOI:10.1016/S0031-9422(99)00348-9

Reference yield:

: 13709-06-3
2,4-bis(methoxymethoxy)benzaldehyde

: 251909-44-1
(E)-1-(4'-O-methoxymethylphenyl)-3-(2'',4''-di-O-methoxymethylphenyl)-propene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 50 percent aq. KOH / ethanol / 0.5 h / 20 °C

1.2: 72 percent / ethanol

2.1: H₂ / 5 percent Pd/C / ethanol / 20 °C

2.2: 99 percent / NaBH₄ / ethanol

3.1: thionyl chloride / CH₂Cl₂ / 0.08 h / 20 °C

4.1: 1,8-DBU / benzene / Heating

With potassium hydroxide; thionyl chloride; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium on activated charcoal; In ethanol; dichloromethane; benzene; 1.1: Metallation / 1.2: Etherification / 2.1: Reduction / 2.2: Reduction / 3.1: Chlorination / 4.1: Elimination;

Reference yield:

: 85699-00-9
1-[4-(methoxymethoxy)phenyl]-1-ethanone

: 251909-44-1
(E)-1-(4'-O-methoxymethylphenyl)-3-(2'',4''-di-O-methoxymethylphenyl)-propene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 50 percent aq. KOH / ethanol / 0.5 h / 20 °C

1.2: 72 percent / ethanol

2.1: H₂ / 5 percent Pd/C / ethanol / 20 °C

2.2: 99 percent / NaBH₄ / ethanol

3.1: thionyl chloride / CH₂Cl₂ / 0.08 h / 20 °C

4.1: 1,8-DBU / benzene / Heating

With potassium hydroxide; thionyl chloride; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium on activated charcoal; In ethanol; dichloromethane; benzene; 1.1: Metallation / 1.2: Etherification / 2.1: Reduction / 2.2: Reduction / 3.1: Chlorination / 4.1: Elimination;