Technology Process of C21H20N6O2
There total 3 articles about C21H20N6O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2,3-Diaminopyridine; C16H13N3O3;
acetic acid;
In
dichloromethane;
at 20 ℃;
for 0.333333h;
With
sodium tris(acetoxy)borohydride;
In
dichloromethane;
at 20 ℃;
for 7h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium tert-butylate / N,N-dimethyl-formamide / 8 h / 65 °C / Inert atmosphere; Cooling with ice
2.1: triethylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C
3.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere
4.1: acetic acid / dichloromethane / 0.33 h / 20 °C
4.2: 7 h / 20 °C
With
potassium tert-butylate; Dess-Martin periodane; triethylamine; HATU;
acetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C
2.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere
3.1: acetic acid / dichloromethane / 0.33 h / 20 °C
3.2: 7 h / 20 °C
With
Dess-Martin periodane; triethylamine; HATU;
acetic acid;
In
dichloromethane; N,N-dimethyl-formamide;