[Co2(CO)4(bis(diphenylphosphino)methane)]-μ,η2,η2-(1,1,1-trifluoro-4-phenylbut-3-yne)

Base Information

Chemical Name:[Co2(CO)4(bis(diphenylphosphino)methane)]-μ,η2,η2-(1,1,1-trifluoro-4-phenylbut-3-yne)
CAS No.:260249-33-0
Molecular Formula:C₃₉H₂₉Co₂F₃O₄P₂
Molecular Weight:798.586
Hs Code.:

Synonyms:[Co2(CO)4(bis(diphenylphosphino)methane)]-μ,η2,η2-(1,1,1-trifluoro-4-phenylbut-3-yne)

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Chemical Property of [Co2(CO)4(bis(diphenylphosphino)methane)]-μ,η2,η2-(1,1,1-trifluoro-4-phenylbut-3-yne)

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Technology Process of [Co2(CO)4(bis(diphenylphosphino)methane)]-μ,η2,η2-(1,1,1-trifluoro-4-phenylbut-3-yne)

There total 5 articles about [Co2(CO)4(bis(diphenylphosphino)methane)]-μ,η2,η2-(1,1,1-trifluoro-4-phenylbut-3-yne) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 260249-28-3
[Co2(CO)4(bis(diphenylphosphino)methane)]-μ,η2,η2-(1,1,1-trifluoro-4-phenylbut-3-yn-2-onium) tetrafluoroborate

: 260249-33-0
[Co2(CO)4(bis(diphenylphosphino)methane)]-μ,η2,η2-(1,1,1-trifluoro-4-phenylbut-3-yne)

Guidance literature:: With Zn; In dichloromethane; under Ar; Co-complex was dissolved in CH2Cl2; excess of Zn was added; stirred for 20 min at room temp.; filtered, solvent was removed under vac., chromy. (silica gel, Et2O/pentane (1/9)); elem. anal.;
DOI:10.1002/(SICI)1099-0682(200002)2000:2<359::AID-EJIC359>3.0.CO;2-V

Reference yield:

: 260249-13-6
[Co2(CO)6]-μ,η2,η2-(1,1,1-trifluoro-4-phenylbut-3-yne-2-ol)

: 260249-33-0
[Co2(CO)4(bis(diphenylphosphino)methane)]-μ,η2,η2-(1,1,1-trifluoro-4-phenylbut-3-yne)

Guidance literature:: Multi-step reaction with 3 steps

1: hexane

2: diethyl ether

3: Zn / dichloromethane

With Zn; In diethyl ether; hexane; dichloromethane;
DOI:10.1002/(SICI)1099-0682(200002)2000:2<359::AID-EJIC359>3.0.CO;2-V

Reference yield:

: 260249-16-9
[Co2(CO)4(bis(diphenylphosphino)methane)]-μ,η2,η2-(1,1,1-trifluoro-4-phenylbut-3-yne-2-ol)

: 260249-33-0
[Co2(CO)4(bis(diphenylphosphino)methane)]-μ,η2,η2-(1,1,1-trifluoro-4-phenylbut-3-yne)

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: Zn / dichloromethane

With Zn; In diethyl ether; dichloromethane;
DOI:10.1002/(SICI)1099-0682(200002)2000:2<359::AID-EJIC359>3.0.CO;2-V