1-(4-(tert-butyl)phenyl)naphthalene

Base Information

• Chemical Name: 1-(4-(tert-butyl)phenyl)naphthalene
• CAS No.: 1233691-86-5
• Molecular Formula: C₂₀H₂₀
• Molecular Weight: 260.379
• Mol file: 1233691-86-5.mol

Synonyms:1-(4-(tert-butyl)phenyl)naphthalene

Chemical Property of 1-(4-(tert-butyl)phenyl)naphthalene

Chemical Property:

Purity/Quality:

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Technology Process of 1-(4-(tert-butyl)phenyl)naphthalene

There total 10 articles about 1-(4-(tert-butyl)phenyl)naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-Naphthylboronic acid (13922-41-3) + 4-tert-butylphenyl mesylate (59970-38-6) → 1-(4-(tert-butyl)phenyl)naphthalene (1233691-86-5)

Guidance literature:

With sodium tetrachloropalladate(II); dicyclohexyl {2-sulfo-9-[3-(4-sulfophenyl)propyl]-9H-fluoren-9-yl}phosphonium hydrogen sulfate; potassium carbonate; In water; at 95 ℃; for 16h; Inert atmosphere;

DOI:10.1002/ejoc.201000251

Reference yield: 96.0%

1-bromo-4-tert-butylbenzene (3972-65-4) + 1-Naphthylboronic acid (13922-41-3) → 1-(4-(tert-butyl)phenyl)naphthalene (1233691-86-5)

Guidance literature:

With potassium phosphate monohydrate; C₃₃H₃₄N₄O₂⁽²⁺⁾*2Br^(1-); palladium diacetate; In tert-butyl alcohol; at 30 ℃; for 24h; Inert atmosphere;

DOI:10.1039/c8ra04094j

Reference yield: 92.0%

N,N,N-trimethyl-1-naphthalenaminium trifluoromethanesulfonate (1351445-39-0) + p-tert-butylphenylboronic acid (123324-71-0) → 1-(4-(tert-butyl)phenyl)naphthalene (1233691-86-5)

Guidance literature:

With SIPr-PdCl₂-Py; cesium fluoride; In tetrahydrofuran; at 80 ℃; for 8h; Schlenk technique; Inert atmosphere;

DOI:10.1016/j.tet.2021.132431

upstream raw materials:

1-Naphthylboronic acid

4-tert-butylphenyl mesylate

1-Bromonaphthalene

p-tert-butylphenylboronic acid