(3β,8α)-9,10-Didehydro-2,3-dihydro-1-<(4-methoxyphenyl)sulfonyl>-6,8-dimethylergoline

Base Information

Chemical Name:(3β,8α)-9,10-Didehydro-2,3-dihydro-1-<(4-methoxyphenyl)sulfonyl>-6,8-dimethylergoline
CAS No.:99499-55-5
Molecular Formula:C₂₃H₂₆N₂O₃S
Molecular Weight:410.537
Hs Code.:

Synonyms:(3β,8α)-9,10-Didehydro-2,3-dihydro-1-<(4-methoxyphenyl)sulfonyl>-6,8-dimethylergoline

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Chemical Property of (3β,8α)-9,10-Didehydro-2,3-dihydro-1-<(4-methoxyphenyl)sulfonyl>-6,8-dimethylergoline

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Technology Process of (3β,8α)-9,10-Didehydro-2,3-dihydro-1-<(4-methoxyphenyl)sulfonyl>-6,8-dimethylergoline

There total 14 articles about (3β,8α)-9,10-Didehydro-2,3-dihydro-1-<(4-methoxyphenyl)sulfonyl>-6,8-dimethylergoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 134745-88-3
(3β,8α,9β)-9-Chloro-2,3-dihydro-1-<(4-methoxyphenyl)sulfonyl>-6,8-dimethylergoline

: 99499-55-5
(3β,8α)-9,10-Didehydro-2,3-dihydro-1-<(4-methoxyphenyl)sulfonyl>-6,8-dimethylergoline

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene; for 40h; Heating;
DOI:10.1248/cpb.39.23

Reference yield: 52.0%

: 99499-54-4
Methanesulfonic acid (5aS,6aR,9R,10R,10aR)-4-(4-methoxy-benzenesulfonyl)-7,9-dimethyl-4,5,5a,6,6a,7,8,9,10,10a-decahydro-indolo[4,3-fg]quinolin-10-yl ester

: 99499-55-5
(3β,8α)-9,10-Didehydro-2,3-dihydro-1-<(4-methoxyphenyl)sulfonyl>-6,8-dimethylergoline

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide;

Reference yield:

: 99499-51-1,99546-35-7,101978-97-6
(3β,8α,9α)-2,3-Dihydro-1-<(4-methoxyphenyl)sulfonyl>-6,8-dimethylergolin-9-ol

: 99499-55-5
(3β,8α)-9,10-Didehydro-2,3-dihydro-1-<(4-methoxyphenyl)sulfonyl>-6,8-dimethylergoline

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / Ambient temperature

2: 52 percent / potassium tert-butoxide / dimethylsulfoxide

With potassium tert-butylate; In pyridine; dimethyl sulfoxide;