bis-pentafluorophenyl 4-pentyloxycarbonylmethoxypyridine-2,6-dicarboxylate

Base Information

Chemical Name:bis-pentafluorophenyl 4-pentyloxycarbonylmethoxypyridine-2,6-dicarboxylate
CAS No.:696609-86-6
Molecular Formula:C₂₆H₁₅F₁₀NO₇
Molecular Weight:643.392
Hs Code.:

Synonyms:bis-pentafluorophenyl 4-pentyloxycarbonylmethoxypyridine-2,6-dicarboxylate

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Chemical Property of bis-pentafluorophenyl 4-pentyloxycarbonylmethoxypyridine-2,6-dicarboxylate

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Technology Process of bis-pentafluorophenyl 4-pentyloxycarbonylmethoxypyridine-2,6-dicarboxylate

There total 7 articles about bis-pentafluorophenyl 4-pentyloxycarbonylmethoxypyridine-2,6-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 696609-79-7
4-pentyloxycarbonylmethoxypyridine-2,6-dicarboxylic acid

: 696609-86-6
bis-pentafluorophenyl 4-pentyloxycarbonylmethoxypyridine-2,6-dicarboxylate

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃;
DOI:10.1039/b315447e

Reference yield:

: 184870-12-0
1,4-dihydro-4-oxopyridine-2,6-dicarbonyl dichloride

: 696609-86-6
bis-pentafluorophenyl 4-pentyloxycarbonylmethoxypyridine-2,6-dicarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1.35 g / i-Pr₂NEt / tetrahydrofuran; dimethylformamide / 60 h / 20 °C

2.1: K₂CO₃ / acetone / 0.75 h / 20 °C

2.2: 97 percent / acetone / 20 °C

3.1: 97 percent / H₂ / Pd/C / ethyl acetate / 20 °C

4.1: 56 percent / DCC; DMAP; i-Pr₂NEt / tetrahydrofuran / 20 °C

With dmap; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1039/b315447e

Reference yield:

: 289038-69-3
4-oxo-1,4-dihydro-pyridine-2,6-dicarboxylic acid dibenzyl ester

: 696609-86-6
bis-pentafluorophenyl 4-pentyloxycarbonylmethoxypyridine-2,6-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: K₂CO₃ / acetone / 0.75 h / 20 °C

1.2: 97 percent / acetone / 20 °C

2.1: 97 percent / H₂ / Pd/C / ethyl acetate / 20 °C

3.1: 56 percent / DCC; DMAP; i-Pr₂NEt / tetrahydrofuran / 20 °C

With dmap; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate; acetone;
DOI:10.1039/b315447e