3-Furancarboxaldehyde, 2-butyltetrahydro-, (2R-trans)- (9CI)

Base Information

Chemical Name:3-Furancarboxaldehyde, 2-butyltetrahydro-, (2R-trans)- (9CI)
CAS No.:175521-61-6
Molecular Formula:C₉H₁₆O₂
Molecular Weight:156.225
Hs Code.:
Mol file:175521-61-6.mol

Synonyms:3-Furancarboxaldehyde, 2-butyltetrahydro-, (2R-trans)- (9CI)

Suppliers and Price of 3-Furancarboxaldehyde, 2-butyltetrahydro-, (2R-trans)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Furancarboxaldehyde, 2-butyltetrahydro-, (2R-trans)- (9CI)

Chemical Property:

PSA：26.30000
LogP:1.78060

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-Furancarboxaldehyde, 2-butyltetrahydro-, (2R-trans)- (9CI)

There total 18 articles about 3-Furancarboxaldehyde, 2-butyltetrahydro-, (2R-trans)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 77733-97-2
2-Butyl-4,5-dihydro-1,3-dioxepin

: 77734-07-7,99487-95-3,99487-99-7,100604-69-1,175521-61-6
(2α,3β)-(+/-)-2-Butyltetrahydro-3-furancarbaldehyd

Guidance literature:: boron trifluoride diethyl etherate; In dichloromethane; at -73 ℃; for 0.5h;
DOI:10.1016/S0040-4039(00)71157-9

Reference yield:

: Trifluoro-methanesulfonic acid (S)-3-phenylethynyl-tetrahydro-furan-2-ylmethyl ester

: 175521-61-6
(2R,3R)-2-Butyl-tetrahydro-furan-3-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / CuBr / tetrahydrofuran / 2 h / 0 °C

2: 98 percent / H₂, ethylenediamine / P-2 nickel / ethanol / 3 h

3: 1.) K₂OsO₄*2H₂O, H₅IO₆, 2.) MeONa / 1.) THF, water, 3 h, 2.) MeOH, 30 min

With potassium osmate(VI); hydrogen; sodium methylate; periodic acid; ethylenediamine; copper(I) bromide; P-2 nickel; In tetrahydrofuran; ethanol;
DOI:10.1016/S0040-4020(96)00058-0

Reference yield:

: Trifluoro-methanesulfonic acid (S)-3-phenylethynyl-tetrahydro-furan-2-ylmethyl ester

: 175521-61-6
(2R,3S)-2-Butyl-tetrahydro-furan-3-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / CuBr / tetrahydrofuran / 2 h / 0 °C

2: 98 percent / H₂, ethylenediamine / P-2 nickel / ethanol / 3 h

3: 1.) K₂OsO₄*2H₂O, H₅IO₆, 2.) MeONa / 1.) THF, water, 3 h, 2.) MeOH, 30 min

With potassium osmate(VI); hydrogen; sodium methylate; periodic acid; ethylenediamine; copper(I) bromide; P-2 nickel; In tetrahydrofuran; ethanol;
DOI:10.1016/S0040-4020(96)00058-0