Technology Process of C23H30N2O2S
There total 6 articles about C23H30N2O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
ethanol;
at 35 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) lithium diisopropylamide / 1) THF, hexane, 1.25 h, -40 deg C; 2) THF, hexane, 0 deg C, 1 h, 40 deg C, 2 h
2: 1.) Mg / 1) THF, 15 deg C, 0.5 h, room temperature, 1 h; 2) THF, overnight, room temperature
3: 99 percent / diethyl ether
4: 91 percent / chromium trioxide, pyridine / Ambient temperature
5: 94 percent / conc. HCl / ethanol / 35 °C
With
pyridine; chromium(VI) oxide; hydrogenchloride; magnesium; lithium diisopropyl amide;
In
diethyl ether; ethanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) Mg / 1) THF, 15 deg C, 0.5 h, room temperature, 1 h; 2) THF, overnight, room temperature
2: 99 percent / diethyl ether
3: 91 percent / chromium trioxide, pyridine / Ambient temperature
4: 94 percent / conc. HCl / ethanol / 35 °C
With
pyridine; chromium(VI) oxide; hydrogenchloride; magnesium;
In
diethyl ether; ethanol;