(4R,5R)-5-benzyloxymethoxy-7-(4-methoxyphenylmethyloxy)-4-methyl-4-(triethylsiloxy)-2-heptynol

Base Information

• Chemical Name: (4R,5R)-5-benzyloxymethoxy-7-(4-methoxyphenylmethyloxy)-4-methyl-4-(triethylsiloxy)-2-heptynol
• CAS No.: 1016985-82-2
• Molecular Formula: C₃₀H₄₄O₆Si
• Molecular Weight: 528.761
• Mol file: 1016985-82-2.mol

Synonyms:(4R,5R)-5-benzyloxymethoxy-7-(4-methoxyphenylmethyloxy)-4-methyl-4-(triethylsiloxy)-2-heptynol

Chemical Property of (4R,5R)-5-benzyloxymethoxy-7-(4-methoxyphenylmethyloxy)-4-methyl-4-(triethylsiloxy)-2-heptynol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (4R,5R)-5-benzyloxymethoxy-7-(4-methoxyphenylmethyloxy)-4-methyl-4-(triethylsiloxy)-2-heptynol

There total 1 articles about (4R,5R)-5-benzyloxymethoxy-7-(4-methoxyphenylmethyloxy)-4-methyl-4-(triethylsiloxy)-2-heptynol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

methyl (4R,5R)-5-benzyloxymethoxy-7-(4-methoxyphenylmethyloxy)-4-methyl-4-(triethylsiloxy)-2-heptynoate (1016985-81-1) → (4R,5R)-5-benzyloxymethoxy-7-(4-methoxyphenylmethyloxy)-4-methyl-4-(triethylsiloxy)-2-heptynol (1016985-82-2)

Guidance literature:

With diisobutylaluminium hydride; In hexane; dichloromethane; at 0 ℃; for 1h;

DOI:10.1021/ol800195g

Reference yield: 99.0%

(4R,5R)-5-benzyloxymethoxy-7-(4-methoxyphenylmethyloxy)-4-methyl-4-(triethylsiloxy)-2-heptynol (1016985-82-2) → (4R,5R)-5-benzyloxymethoxy-7-(4-methoxyphenylmethyloxy)-4-methylhept-2-yne-1,4-diol (1016985-83-3)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 16h;

DOI:10.1021/ol800195g

upstream raw materials:

methyl (4R,5R)-5-benzyloxymethoxy-7-(4-methoxyphenylmethyloxy)-4-methyl-4-(triethylsiloxy)-2-heptynoate

Downstream raw materials:

(4R,5R)-5-benzyloxymethoxy-7-(4-methoxyphenylmethyloxy)-4-methylhept-2-yne-1,4-diol