methyl 4-azido-6-O-triphenylmethyl-2,3,4-trideoxy-D-threo-hexopyranoside

Base Information

Chemical Name:methyl 4-azido-6-O-triphenylmethyl-2,3,4-trideoxy-D-threo-hexopyranoside
CAS No.:904304-41-2
Molecular Formula:C₂₆H₂₇N₃O₃
Molecular Weight:429.519
Hs Code.:

Synonyms:methyl 4-azido-6-O-triphenylmethyl-2,3,4-trideoxy-D-threo-hexopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-azido-6-O-triphenylmethyl-2,3,4-trideoxy-D-threo-hexopyranoside

Chemical Property:

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Technology Process of methyl 4-azido-6-O-triphenylmethyl-2,3,4-trideoxy-D-threo-hexopyranoside

There total 5 articles about methyl 4-azido-6-O-triphenylmethyl-2,3,4-trideoxy-D-threo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 904304-40-1
methyl 4-O-methanesulfonyl-6-O-triphenylmethyl-2,3-dideoxy-D-erythro-hexopyranoside

: 904304-41-2
methyl 4-azido-6-O-triphenylmethyl-2,3,4-trideoxy-D-threo-hexopyranoside

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 110 ℃; for 6h;
DOI:10.3390/10080871

Reference yield:

: 3427-20-1
methyl 4,6-di-O-acetyl-2,3-dideoxy-D-erythro-hex-2-enopyranoside

: 904304-41-2
methyl 4-azido-6-O-triphenylmethyl-2,3,4-trideoxy-D-threo-hexopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / H₂ / Pd/C / methanol / 1 h / 20 °C

2: 90 percent / Na₂CO₃ / methanol / 3 h / 20 °C

3: 70 percent / Et₃N; DMAP / dimethylformamide / 36 h / 20 °C

4: 87 percent / Et₃N / CH₂Cl₂ / 1.5 h / 20 °C

5: 90 percent / aq. sodium azide / dimethylformamide / 6 h / 110 °C

With dmap; sodium azide; hydrogen; sodium carbonate; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.3390/10080871

Reference yield:

: 904304-39-8
methyl 6-O-triphenylmethyl-2,3-dideoxy-D-erythro-hexopyranoside

: 904304-41-2
methyl 4-azido-6-O-triphenylmethyl-2,3,4-trideoxy-D-threo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / Et₃N / CH₂Cl₂ / 1.5 h / 20 °C

2: 90 percent / aq. sodium azide / dimethylformamide / 6 h / 110 °C

With sodium azide; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.3390/10080871