(+)-(2R,3R)-2-ethyl-2-methyl-4-nitro-3-phenyl-butyraldehyde

Base Information

• Chemical Name: (+)-(2R,3R)-2-ethyl-2-methyl-4-nitro-3-phenyl-butyraldehyde
• CAS No.: 748807-19-4
• Molecular Formula: C₁₃H₁₇NO₃
• Molecular Weight: 235.283
• Mol file: 748807-19-4.mol

Synonyms:(+)-(2R,3R)-2-ethyl-2-methyl-4-nitro-3-phenyl-butyraldehyde

Chemical Property of (+)-(2R,3R)-2-ethyl-2-methyl-4-nitro-3-phenyl-butyraldehyde

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (+)-(2R,3R)-2-ethyl-2-methyl-4-nitro-3-phenyl-butyraldehyde

There total 1 articles about (+)-(2R,3R)-2-ethyl-2-methyl-4-nitro-3-phenyl-butyraldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

nitrostyrene (5153-67-3) + 2-Methylbutyraldehyde (96-17-3,57456-98-1) → (+)-(2R,3R)-2-ethyl-2-methyl-4-nitro-3-phenyl-butyraldehyde (748807-19-4) + (2R,3S)-2-ethyl-2-methyl-4-nitro-3-phenyl-butyraldehyde + (2S,3R)-2-ethyl-2-methyl-4-nitro-3-phenyl-butyraldehyde + (-)-(2S,3S)-2-ethyl-2-methyl-4-nitro-3-phenyl-butyraldehyde

Guidance literature:

With (S)-2-(1-pyrrolidinylmethyl)pyrrolidine; trifluoroacetic acid; In isopropyl alcohol; at 4 ℃; for 96h; Title compound not separated from byproducts;

DOI:10.1021/ol049196o

Reference yield:

(2,4-dinitro-phenyl)-hydrazine (119-26-6) + (+)-(2R,3R)-2-ethyl-2-methyl-4-nitro-3-phenyl-butyraldehyde (748807-19-4) → N-(2,4-dinitrophenyl)-N'-(2-ethyl-2-methyl-4-nitro-3-phenylbutylidene)hydazine

Guidance literature:

With sulfuric acid; In methanol; ethanol; water; at 20 ℃; for 0.0833333h;

DOI:10.1021/ol049196o

upstream raw materials:

nitrostyrene

2-Methylbutyraldehyde