Technology Process of C16H20O3
There total 10 articles about C16H20O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
C38H39IrNOP(1+)*C32H12BF24(1-); hydrogen;
In
dichloromethane;
at 20 ℃;
for 10h;
under 22801.5 Torr;
Inert atmosphere;
Glovebox;
Autoclave;
DOI:10.1002/anie.201309521
- Guidance literature:
-
With
C39H41IrNOP(1+)*C32H12BF24(1-); hydrogen;
In
dichloromethane;
at 20 ℃;
for 10h;
under 22801.5 Torr;
Overall yield = 97 %;
Inert atmosphere;
Glovebox;
Autoclave;
DOI:10.1002/anie.201309521
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: XPhos; tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butoxide / 1,4-dioxane / 0.17 h / Inert atmosphere
1.2: 5 h / 110 °C / Inert atmosphere
2.1: lithium hydroxide / tetrahydrofuran; water / 5 h / 60 °C
3.1: triethylamine; hydrogen; C38H39IrNOP(1+)*C32H12BF24(1-) / dichloromethane / 10 h / 20 °C / 22801.5 Torr / Inert atmosphere; Glovebox; Autoclave
4.1: hydrogen; C38H39IrNOP(1+)*C32H12BF24(1-) / dichloromethane / 10 h / 20 °C / 22801.5 Torr / Inert atmosphere; Glovebox; Autoclave
With
tris-(dibenzylideneacetone)dipalladium(0); C38H39IrNOP(1+)*C32H12BF24(1-); hydrogen; triethylamine; lithium hydroxide; lithium tert-butoxide; XPhos;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1002/anie.201309521
