(E)-4-((4-(1,4,8,11-tetraazacyclotetradecan-1-ylsulfonyl)phenyl)diazenyl)-N,N-dimethylaniline

Base Information

• Chemical Name: (E)-4-((4-(1,4,8,11-tetraazacyclotetradecan-1-ylsulfonyl)phenyl)diazenyl)-N,N-dimethylaniline
• CAS No.: 1262862-09-8
• Molecular Formula: C₂₄H₃₇N₇O₂S
• Molecular Weight: 487.669

Synonyms:(E)-4-((4-(1,4,8,11-tetraazacyclotetradecan-1-ylsulfonyl)phenyl)diazenyl)-N,N-dimethylaniline

Chemical Property of (E)-4-((4-(1,4,8,11-tetraazacyclotetradecan-1-ylsulfonyl)phenyl)diazenyl)-N,N-dimethylaniline

Chemical Property:

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Technology Process of (E)-4-((4-(1,4,8,11-tetraazacyclotetradecan-1-ylsulfonyl)phenyl)diazenyl)-N,N-dimethylaniline

There total 1 articles about (E)-4-((4-(1,4,8,11-tetraazacyclotetradecan-1-ylsulfonyl)phenyl)diazenyl)-N,N-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

1,4,8,11-Tetraazacyclotetradecane (295-37-4) + (E)-4-((4-(dimethylamino)phenyl)diazenyl)benzene-1-sulfonyl chloride → (E)-4-((4-(1,4,8,11-tetraazacyclotetradecan-1-ylsulfonyl)phenyl)diazenyl)-N,N-dimethylaniline (1262862-09-8)

Guidance literature:

With 2-amino-3,3-dimethylbutane; In tetrahydrofuran; at 25 ℃; for 11h; Reflux;

DOI:10.1039/c0cc01996h

Reference yield: 65.0%

(E)-4-((4-(1,4,8,11-tetraazacyclotetradecan-1-ylsulfonyl)phenyl)diazenyl)-N,N-dimethylaniline (1262862-09-8) + zinc nitrate → C24H34N7O2SZn(2+)

Guidance literature:

In methanol; at 25 ℃; for 15h; Product distribution / selectivity;

Reference yield: 65.0%

zinc(II) nitrate hexahydrate + (E)-4-((4-(1,4,8,11-tetraazacyclotetradecan-1-ylsulfonyl)phenyl)diazenyl)-N,N-dimethylaniline (1262862-09-8) → [Zn((E)-4-((4-(1,4,8,11-tetraazacyclotetradecan-1-ylsulfonyl)phenyl)diazenyl)-N,N-dimethylaniline)(H2O)2](2+)

Guidance literature:

In methanol; for 2 h at 25°C;

DOI:10.1021/ic200223g

upstream raw materials:

1,4,8,11-Tetraazacyclotetradecane

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