N-[Amino(imino)methyl]-4-methylpiperazine-1-carboximidamide

Base Information

• Chemical Name: N-[Amino(imino)methyl]-4-methylpiperazine-1-carboximidamide
• CAS No.: 18413-26-8
• Molecular Formula: C₇H₁₆N₆
• Molecular Weight: 184.244
• Mol file: 18413-26-8.mol

Synonyms:4-methylpiperazin-1-yl-biguanidine dihydrochloride

Chemical Property of N-[Amino(imino)methyl]-4-methylpiperazine-1-carboximidamide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

N-[Amino(imino)methyl]-4-methylpiperazine-1-carboximidamide ^*data from reagent suppliers

Safty Information:

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Technology Process of N-[Amino(imino)methyl]-4-methylpiperazine-1-carboximidamide

There total 3 articles about N-[Amino(imino)methyl]-4-methylpiperazine-1-carboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

1-methyl-piperazine (109-01-3) + N-Cyanoguanidine (127099-85-8,780722-26-1,461-58-5) → 4-methylpiperazin-1-yl-biguanidine dihydrochloride (18413-26-8)

Guidance literature:

1-methyl-piperazine; N-Cyanoguanidine; In toluene; at 20 ℃; for 0.25h;

With hydrogenchloride; In water; toluene; for 7h;

DOI:10.1155/2017/1212609

Reference yield:

N-methylpiperazine dihydrochloride (50398-09-9,51545-09-6,34352-59-5) + N-Cyanoguanidine (127099-85-8,780722-26-1,461-58-5) → 4-methylpiperazin-1-yl-biguanidine dihydrochloride (18413-26-8)

Guidance literature:

at 150 ℃;

DOI:10.1021/ja01523a059

Reference yield:

→ 4-methylpiperazin-1-yl-biguanidine dihydrochloride (18413-26-8)

Guidance literature:

N-Methyl-piperazin-hydrochlorid, Dicyanamid,(Schmelzen);

upstream raw materials:

N-methylpiperazine dihydrochloride

N-Cyanoguanidine

1-methyl-piperazine

Downstream raw materials:

(4-(4-bromophenyl)-6-(4-methylpiperazin-1-yl)-1,3,5-triazin-2-amine)

4-(4-methylpiperazin-1-yl)-6-(4-cyanophenyl)-1,3,5-triazin-2-amine

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