Trichloroacetimidate 2,3,6-tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-α/β-D-galactopyranosyl)-α/β-D-glucopyranoside

Base Information

Chemical Name:Trichloroacetimidate 2,3,6-tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-α/β-D-galactopyranosyl)-α/β-D-glucopyranoside
CAS No.:473449-32-0
Molecular Formula:C₆₃H₅₀Cl₃NO₁₈
Molecular Weight:1215.44
Hs Code.:

Synonyms:Trichloroacetimidate 2,3,6-tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-α/β-D-galactopyranosyl)-α/β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Trichloroacetimidate 2,3,6-tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-α/β-D-galactopyranosyl)-α/β-D-glucopyranoside

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Technology Process of Trichloroacetimidate 2,3,6-tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-α/β-D-galactopyranosyl)-α/β-D-glucopyranoside

There total 5 articles about Trichloroacetimidate 2,3,6-tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-α/β-D-galactopyranosyl)-α/β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: C₆₈H₅₄O₂₀

: 545-06-2
trichloroacetonitrile

: 473449-32-0
Trichloroacetimidate 2,3,6-tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-α/β-D-galactopyranosyl)-α/β-D-glucopyranoside

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c8ob01087k

Reference yield: 72.0%

: 140209-81-0
2,3,6-Tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-α/β-D-glucopyranose

: 545-06-2
trichloroacetonitrile

: 473449-32-0
Trichloroacetimidate 2,3,6-tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-α/β-D-galactopyranosyl)-α/β-D-glucopyranoside

Guidance literature:: With sodium hydride; In dichloromethane; at 0 ℃; for 4h;
DOI:10.1016/S0040-4020(01)88191-6

Reference yield: 29.0%

: 91280-47-6
2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->4)-1,2,3,6-tetra-O-benzoyl-D-glucopyranose

: 545-06-2
trichloroacetonitrile

: 473449-32-0
Trichloroacetimidate 2,3,6-tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-α/β-D-galactopyranosyl)-α/β-D-glucopyranoside

Guidance literature:: 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->4)-1,2,3,6-tetra-O-benzoyl-D-glucopyranose; With dimethyl amine; In pyridine; ethanol; at 0 - 20 ℃; for 2h;

trichloroacetonitrile; With potassium carbonate; In dichloromethane; at 0 - 20 ℃; for 2h; Molecular sieve;