8-methoxycarbonyloct-1-yl 4-O-(4,6-O-cyclohexylidene-2-O-(2,6-di-O-acetyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-α-D-mannopyranosyl)-2,3-di-O-acetyl-α-L-rhamnopyranoside

Base Information

Chemical Name:8-methoxycarbonyloct-1-yl 4-O-(4,6-O-cyclohexylidene-2-O-(2,6-di-O-acetyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-α-D-mannopyranosyl)-2,3-di-O-acetyl-α-L-rhamnopyranoside
CAS No.:91887-39-7
Molecular Formula:C₅₆H₇₄O₂₃
Molecular Weight:1115.19
Hs Code.:

8-methoxycarbonyloct-1-yl 4-O-(4,6-O-cyclohexylidene-2-O-(2,6-di-O-acetyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-α-D-mannopyranosyl)-2,3-di-O-acetyl-α-L-rhamnopyranoside

Synonyms:8-methoxycarbonyloct-1-yl 4-O-(4,6-O-cyclohexylidene-2-O-(2,6-di-O-acetyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-α-D-mannopyranosyl)-2,3-di-O-acetyl-α-L-rhamnopyranoside

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Chemical Property of 8-methoxycarbonyloct-1-yl 4-O-(4,6-O-cyclohexylidene-2-O-(2,6-di-O-acetyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-α-D-mannopyranosyl)-2,3-di-O-acetyl-α-L-rhamnopyranoside

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Technology Process of 8-methoxycarbonyloct-1-yl 4-O-(4,6-O-cyclohexylidene-2-O-(2,6-di-O-acetyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-α-D-mannopyranosyl)-2,3-di-O-acetyl-α-L-rhamnopyranoside

There total 10 articles about 8-methoxycarbonyloct-1-yl 4-O-(4,6-O-cyclohexylidene-2-O-(2,6-di-O-acetyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-α-D-mannopyranosyl)-2,3-di-O-acetyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1122-84-5
1-ethoxycyclohexene

: C₅₀H₆₆O₂₃

: 91887-39-7
8-methoxycarbonyloct-1-yl 4-O-(4,6-O-cyclohexylidene-2-O-(2,6-di-O-acetyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-α-D-mannopyranosyl)-2,3-di-O-acetyl-α-L-rhamnopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In acetonitrile; at 0 ℃; for 0.116667h;

Reference yield:

: 65827-59-0
2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl chloride

: 91887-39-7
8-methoxycarbonyloct-1-yl 4-O-(4,6-O-cyclohexylidene-2-O-(2,6-di-O-acetyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-α-D-mannopyranosyl)-2,3-di-O-acetyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 9 steps

1: 79 percent / silver trifluoromethanesulfonate, molecular sieves / toluene; nitromethane / 0.5 h / -40 °C

2: 95 percent / sodium methoxide / methanol / 3 h / 30 °C

3: 88 percent / silver trifluoromethanesulfonate, molecular sieves / toluene; nitromethane / 0.75 h / -30 °C

4: 1,8-diaza-<2.2.2.>-bicyclooctane, tris (triphenylphosphine)rhodium chloride / ethanol; H₂O; toluene / 3.5 h / Heating

5: red mercury(II) oxide, mercury(II) chloride / acetone; H₂O / 7 h / Ambient temperature

6: acetic acid, water / 27 h / 60 °C

7: pyridine, 4-dimethylaminopyridine / Ambient temperature

8: 100 percent / H₂ / Pd/C / methanol; acetic acid / 24 h / 735.5 Torr

9: 92 percent / p-toluenesulfonic acid / acetonitrile / 0.12 h / 0 °C

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; dmap; Wilkinson's catalyst; molecular sieve; water; hydrogen; sodium methylate; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; acetic acid; mercury dichloride; mercury(II) oxide; palladium on activated charcoal; In methanol; nitromethane; ethanol; water; acetic acid; acetone; toluene; acetonitrile;

Reference yield:

: 91887-38-6
8-methoxycarbonyloct-1-yl 2,3-di-O-acetyl-4-O-(2-O-(2,6-di-O-acetyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-2,3-O-cyclohexylidene-α-L-rhamnopyranoside

: 91887-39-7
8-methoxycarbonyloct-1-yl 4-O-(4,6-O-cyclohexylidene-2-O-(2,6-di-O-acetyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-α-D-mannopyranosyl)-2,3-di-O-acetyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / Pd/C / methanol; acetic acid / 24 h / 735.5 Torr

2: 92 percent / p-toluenesulfonic acid / acetonitrile / 0.12 h / 0 °C

With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; acetic acid; acetonitrile;