Technology Process of NHC4Br(C6H4Br)2NC4N(C6H4Br)2Br
There total 5 articles about NHC4Br(C6H4Br)2NC4N(C6H4Br)2Br which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-Bromosuccinimide;
In
dichloromethane;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/ic300709n
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonium acetate / butan-1-ol / 24 h / Reflux
2: N-Bromosuccinimide / dichloromethane / 20 °C / Inert atmosphere
With
N-Bromosuccinimide; ammonium acetate;
In
dichloromethane; butan-1-ol;
DOI:10.1021/ic300709n
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium hydroxide / ethanol; water
2: diethylamine / methanol / 24 h / Reflux
3: ammonium acetate / butan-1-ol / 24 h / Reflux
4: N-Bromosuccinimide / dichloromethane / 20 °C / Inert atmosphere
With
N-Bromosuccinimide; ammonium acetate; diethylamine; potassium hydroxide;
In
methanol; ethanol; dichloromethane; water; butan-1-ol;
DOI:10.1021/ic300709n
