Technology Process of C24H25N3O7S
There total 6 articles about C24H25N3O7S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; dimethyl sulfide borane;
In
tetrahydrofuran;
at 23 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/ol302077n
- Guidance literature:
-
Multi-step reaction with 5 steps
1.2: 1.08 h / 0 - 20 °C / Inert atmosphere
2.1: tributylphosphine / 20 °C / Inert atmosphere
3.1: silica gel / toluene / 5 h / Inert atmosphere; Reflux
4.1: tetrahydrofuran / 0 - 23 °C / Inert atmosphere
5.1: dimethyl sulfide borane; water / tetrahydrofuran / 2 h / 23 °C / Inert atmosphere
With
tributylphosphine; water; dimethyl sulfide borane;
In
tetrahydrofuran; toluene;
DOI:10.1021/ol302077n
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tributylphosphine / 20 °C / Inert atmosphere
2: silica gel / toluene / 5 h / Inert atmosphere; Reflux
3: tetrahydrofuran / 0 - 23 °C / Inert atmosphere
4: dimethyl sulfide borane; water / tetrahydrofuran / 2 h / 23 °C / Inert atmosphere
With
tributylphosphine; water; dimethyl sulfide borane;
In
tetrahydrofuran; toluene;
DOI:10.1021/ol302077n