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C37H50N4O6

Base Information
  • Chemical Name:C37H50N4O6
  • CAS No.:944140-64-1
  • Molecular Formula:C37H50N4O6
  • Molecular Weight:646.827
  • Hs Code.:
C<sub>37</sub>H<sub>50</sub>N<sub>4</sub>O<sub>6</sub>

Synonyms:C37H50N4O6

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Chemical Property of C37H50N4O6
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Technology Process of C37H50N4O6

There total 13 articles about C37H50N4O6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 3h;
DOI:10.1021/ml500137b
Guidance literature:
Multi-step reaction with 7 steps
1: sodium hydrogencarbonate / water; tetrahydrofuran / 20 °C / Large scale
2: potassium carbonate / water; methanol / 96 h / Reflux
3: acetic anhydride / 4.5 h / Reflux
4: hydroquinine (anthraquinone-1,4-diyl) diether / tetrahydrofuran; diethyl ether / -78 - 20 °C
5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole / N,N-dimethyl-formamide / 20 h / 20 °C
6: lithium hydroxide monohydrate / water; tetrahydrofuran / 3 h / 0 - 20 °C
7: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole / N,N-dimethyl-formamide / 3 h / 20 °C
With 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; sodium hydrogencarbonate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinine (anthraquinone-1,4-diyl) diether; In tetrahydrofuran; methanol; diethyl ether; water; acetic anhydride; N,N-dimethyl-formamide;
DOI:10.1021/ml500137b
Guidance literature:
Multi-step reaction with 8 steps
1: acetic acid; platinum(IV) oxide; hydrogen / 27 h / 24 °C / 3750.38 Torr / Autoclave; Large scale
2: sodium hydrogencarbonate / water; tetrahydrofuran / 20 °C / Large scale
3: potassium carbonate / water; methanol / 96 h / Reflux
4: acetic anhydride / 4.5 h / Reflux
5: hydroquinine (anthraquinone-1,4-diyl) diether / tetrahydrofuran; diethyl ether / -78 - 20 °C
6: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole / N,N-dimethyl-formamide / 20 h / 20 °C
7: lithium hydroxide monohydrate / water; tetrahydrofuran / 3 h / 0 - 20 °C
8: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole / N,N-dimethyl-formamide / 3 h / 20 °C
With platinum(IV) oxide; 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; hydrogen; sodium hydrogencarbonate; potassium carbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinine (anthraquinone-1,4-diyl) diether; In tetrahydrofuran; methanol; diethyl ether; water; acetic anhydride; N,N-dimethyl-formamide;
DOI:10.1021/ml500137b
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