C₁₄H₁₆INO

Base Information

Chemical Name:C₁₄H₁₆INO
CAS No.:1454769-88-0
Molecular Formula:C₁₄H₁₆INO
Molecular Weight:341.192
Hs Code.:

Synonyms:C₁₄H₁₆INO

Suppliers and Price of C₁₄H₁₆INO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₆INO

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₁₄H₁₆INO

There total 4 articles about C₁₄H₁₆INO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 615-43-0
2-iodophenylamine

: 1454769-87-9
C₈H₁₁ClO

: 1454769-88-0
C₁₄H₁₆INO

Guidance literature:: With dmap; triethylamine; In dichloromethane; at -20 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol402210a

Reference yield:

: 112391-42-1
dimethyl 2-(3-methylbut-3-enyl)propane-1,3-dioate

: 1454769-88-0
C₁₄H₁₆INO

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide; water / methanol / 1 h / Inert atmosphere; Reflux

2: diethylamine / ethyl acetate / 2 h / Inert atmosphere; Reflux

3: thionyl chloride / 0.5 h / 80 °C

4: dmap; triethylamine / dichloromethane / -20 - 20 °C / Inert atmosphere

With dmap; thionyl chloride; water; diethylamine; triethylamine; sodium hydroxide; In methanol; dichloromethane; ethyl acetate;
DOI:10.1021/ol402210a

Reference yield:

: 343271-32-9
2-(3-methyl-3-buten-1-yl)malonic acid

: 1454769-88-0
C₁₄H₁₆INO

Guidance literature:: Multi-step reaction with 3 steps

1: diethylamine / ethyl acetate / 2 h / Inert atmosphere; Reflux

2: thionyl chloride / 0.5 h / 80 °C

3: dmap; triethylamine / dichloromethane / -20 - 20 °C / Inert atmosphere

With dmap; thionyl chloride; diethylamine; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1021/ol402210a