3-cyclohexen-1-one cyclic (1S,2S)-1,2-bis-<(benzyloxy)methyl>ethylene acetal

Base Information

• Chemical Name: 3-cyclohexen-1-one cyclic (1S,2S)-1,2-bis-<(benzyloxy)methyl>ethylene acetal
• CAS No.: 99249-37-3
• Molecular Formula: C₂₄H₂₈O₄
• Molecular Weight: 380.484

Synonyms:3-cyclohexen-1-one cyclic (1S,2S)-1,2-bis-<(benzyloxy)methyl>ethylene acetal

Chemical Property of 3-cyclohexen-1-one cyclic (1S,2S)-1,2-bis-<(benzyloxy)methyl>ethylene acetal

Chemical Property:

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Technology Process of 3-cyclohexen-1-one cyclic (1S,2S)-1,2-bis-<(benzyloxy)methyl>ethylene acetal

There total 4 articles about 3-cyclohexen-1-one cyclic (1S,2S)-1,2-bis-<(benzyloxy)methyl>ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2S,3S)-1,4-bis(benzyloxy)-2,3-butanediol (17401-06-8) → 3-cyclohexen-1-one cyclic (1S,2S)-1,2-bis-<(benzyloxy)methyl>ethylene acetal (99249-37-3)

Guidance literature:

DOI:10.1021/ja00312a073

Reference yield:

(2S,3S)-1,4-bis(benzyloxy)-2,3-butanediol (17401-06-8) + 4-oxocyclohexyl 4-methylbenzenesulfonate (23511-04-8) → 3-cyclohexen-1-one cyclic (1S,2S)-1,2-bis-<(benzyloxy)methyl>ethylene acetal (99249-37-3)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1016/S0040-4020(01)90002-X

Reference yield:

Toluene-4-sulfonic acid (2S,3S)-2,3-bis-benzyloxymethyl-1,4-dioxa-spiro[4.5]dec-8-yl ester → 3-cyclohexen-1-one cyclic (1S,2S)-1,2-bis-<(benzyloxy)methyl>ethylene acetal (99249-37-3)

Guidance literature:

Yield given;

DOI:10.1021/ja00312a073

upstream raw materials:

(2S,3S)-1,4-bis(benzyloxy)-2,3-butanediol

4-oxocyclohexyl 4-methylbenzenesulfonate

Downstream raw materials:

3-norcaranone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

3-norcaranone cyclic <1S,2S>-1,2-bis<(benzyloxy)methyl>ethylene acetal

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