N₁,N₃-bis[3,5-bis(trifluoromethyl)phenyl]-2-(9-ethyl-9H-purin-6-yl)benzene-1,3-diamine

Base Information

• Chemical Name: N₁,N₃-bis[3,5-bis(trifluoromethyl)phenyl]-2-(9-ethyl-9H-purin-6-yl)benzene-1,3-diamine
• CAS No.: 1535484-05-9
• Molecular Formula: C₂₉H₁₈F₁₂N₆
• Molecular Weight: 678.483

Synonyms:N₁,N₃-bis[3,5-bis(trifluoromethyl)phenyl]-2-(9-ethyl-9H-purin-6-yl)benzene-1,3-diamine

Chemical Property of N₁,N₃-bis[3,5-bis(trifluoromethyl)phenyl]-2-(9-ethyl-9H-purin-6-yl)benzene-1,3-diamine

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Technology Process of N₁,N₃-bis[3,5-bis(trifluoromethyl)phenyl]-2-(9-ethyl-9H-purin-6-yl)benzene-1,3-diamine

There total 2 articles about N₁,N₃-bis[3,5-bis(trifluoromethyl)phenyl]-2-(9-ethyl-9H-purin-6-yl)benzene-1,3-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3,5-bis(trifluoromethyl)phenyl azide + N-[2-(9-ethyl-9H-purin-6-yl)phenyl]-3,5-bis(trifluoromethyl)aniline (1535484-04-8) → N1,N3-bis[3,5-bis(trifluoromethyl)phenyl]-2-(9-ethyl-9H-purin-6-yl)benzene-1,3-diamine (1535484-05-9)

Guidance literature:

With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; In 1,2-dichloro-ethane; at 85 ℃; for 12h;

DOI:10.1021/ja4118472

Reference yield: 84.0%

3,5-bis(trifluoromethyl)phenyl azide + 9-ethyl-6-phenyl-9H-purine (83026-89-5) → N1,N3-bis[3,5-bis(trifluoromethyl)phenyl]-2-(9-ethyl-9H-purin-6-yl)benzene-1,3-diamine (1535484-05-9)

Guidance literature:

With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; In 1,2-dichloro-ethane; at 85 ℃; for 24h;

DOI:10.1021/ja4118472

upstream raw materials:

N-[2-(9-ethyl-9H-purin-6-yl)phenyl]-3,5-bis(trifluoromethyl)aniline

9-ethyl-6-phenyl-9H-purine

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