(+/-)-2-(N,N'-bis(t-butoxycarbonyl)hydrazino)-3-phenylpropanoic acid benzyl ester

Base Information

Chemical Name:(+/-)-2-(N,N'-bis(t-butoxycarbonyl)hydrazino)-3-phenylpropanoic acid benzyl ester
CAS No.:120020-02-2
Molecular Formula:C₂₆H₃₄N₂O₆
Molecular Weight:470.566
Hs Code.:

Synonyms:(+/-)-2-(N,N'-bis(t-butoxycarbonyl)hydrazino)-3-phenylpropanoic acid benzyl ester

Suppliers and Price of (+/-)-2-(N,N'-bis(t-butoxycarbonyl)hydrazino)-3-phenylpropanoic acid benzyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+/-)-2-(N,N'-bis(t-butoxycarbonyl)hydrazino)-3-phenylpropanoic acid benzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-2-(N,N'-bis(t-butoxycarbonyl)hydrazino)-3-phenylpropanoic acid benzyl ester

There total 7 articles about (+/-)-2-(N,N'-bis(t-butoxycarbonyl)hydrazino)-3-phenylpropanoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 15082-42-5
lithium benzyloxide

: C₂₅H₃₇N₃O₇

: 120020-02-2
(+/-)-2-(N,N'-bis(t-butoxycarbonyl)hydrazino)-3-phenylpropanoic acid benzyl ester

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 0.25h;
DOI:10.1021/ja00280a051

Reference yield: 56.0%

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 22767-96-0
Benzyl 3-phenylpropionate

: 120020-02-2
(+/-)-2-(N,N'-bis(t-butoxycarbonyl)hydrazino)-3-phenylpropanoic acid benzyl ester

Guidance literature:: Benzyl 3-phenylpropionate; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

di-tert-butyl-diazodicarboxylate; In tetrahydrofuran; hexane; dichloromethane; at -78 - 20 ℃;
DOI:10.1016/S0040-4020(00)00923-6

Reference yield:

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 120020-02-2
(+/-)-2-(N,N'-bis(t-butoxycarbonyl)hydrazino)-3-phenylpropanoic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LDA / 1.) THF, -78 degC; 2.) THF, -78 degC

2: 97 percent / tetrahydrofuran / 0.25 h / 0 °C

With lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/ja00280a051