tert-butyldimethylsilyl 2-azido-6-O-benzyl-2-deoxy-3-O-fluorenylmethoxycarbonyl-β-D-galactopyranoside

Base Information

Chemical Name:tert-butyldimethylsilyl 2-azido-6-O-benzyl-2-deoxy-3-O-fluorenylmethoxycarbonyl-β-D-galactopyranoside
CAS No.:1218904-35-8
Molecular Formula:C₃₄H₄₁N₃O₇Si
Molecular Weight:631.801
Hs Code.:

Synonyms:tert-butyldimethylsilyl 2-azido-6-O-benzyl-2-deoxy-3-O-fluorenylmethoxycarbonyl-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyldimethylsilyl 2-azido-6-O-benzyl-2-deoxy-3-O-fluorenylmethoxycarbonyl-β-D-galactopyranoside

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Technology Process of tert-butyldimethylsilyl 2-azido-6-O-benzyl-2-deoxy-3-O-fluorenylmethoxycarbonyl-β-D-galactopyranoside

There total 1 articles about tert-butyldimethylsilyl 2-azido-6-O-benzyl-2-deoxy-3-O-fluorenylmethoxycarbonyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1218904-43-8
tert-butyldimethylsilyl 2-azido-4,6-benzylidene-2-deoxy-3-O-fluorenylmethoxycarbonyl-β-D-galactopyranoside

: 1218904-35-8
tert-butyldimethylsilyl 2-azido-6-O-benzyl-2-deoxy-3-O-fluorenylmethoxycarbonyl-β-D-galactopyranoside

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane; at 0 - 23 ℃; Inert atmosphere;
DOI:10.1021/ol1003912

Reference yield: 59.0%

: 1218904-29-0
3-O-acetyl-2-azido-4-(benzyloxycarbonyl)amino-2,4,6-dideoxy-D-galactopyranosyl N-phenyltrifluoroacetimidate

: 1218904-35-8
tert-butyldimethylsilyl 2-azido-6-O-benzyl-2-deoxy-3-O-fluorenylmethoxycarbonyl-β-D-galactopyranoside

: C₅₀H₅₉N₇O₁₂Si

: 1218904-38-1
C₅₀H₅₉N₇O₁₂Si

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol1003912