N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(3-(4-methylpiperazin-1-yl)phenyl)acetamide)

Base Information

Chemical Name:N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(3-(4-methylpiperazin-1-yl)phenyl)acetamide)
CAS No.:1610728-52-3
Molecular Formula:C₃₆H₄₆N₁₀O₂S₂
Molecular Weight:714.959
Hs Code.:

Synonyms:N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(3-(4-methylpiperazin-1-yl)phenyl)acetamide)

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Chemical Property of N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(3-(4-methylpiperazin-1-yl)phenyl)acetamide)

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Technology Process of N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(3-(4-methylpiperazin-1-yl)phenyl)acetamide)

There total 3 articles about N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(3-(4-methylpiperazin-1-yl)phenyl)acetamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1191399-65-1
[3-(4-methylpiperazin-1-yl)phenyl]acetic acid methyl ester

: 1610728-92-1
5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazol-2-amine)

: 1610728-52-3
N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(3-(4-methylpiperazin-1-yl)phenyl)acetamide)

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; at 100 ℃; for 0.666667h; Inert atmosphere; Microwave irradiation;

Reference yield:

: 2305-30-8,2305-31-9,3971-31-1,21917-23-7,116724-13-1,116724-14-2
trans-e,a-1,3-cyclohexanedicarboxylic acid

: 1610728-52-3
N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(3-(4-methylpiperazin-1-yl)phenyl)acetamide)

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 3 h / 40 - 80 °C

2: potassium tert-butylate / dimethyl sulfoxide / 0.67 h / 100 °C / Inert atmosphere; Microwave irradiation

With potassium tert-butylate; trichlorophosphate; In dimethyl sulfoxide;

Reference yield:

: 1610728-91-0
(S,S)-dibenzyl cyclohexyl 1,3-dicarboxylate

: 1610728-52-3
N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(3-(4-methylpiperazin-1-yl)phenyl)acetamide)

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 0.33 h

2: trichlorophosphate / 3 h / 40 - 80 °C

3: potassium tert-butylate / dimethyl sulfoxide / 0.67 h / 100 °C / Inert atmosphere; Microwave irradiation

With palladium 10% on activated carbon; potassium tert-butylate; hydrogen; trichlorophosphate; In methanol; dimethyl sulfoxide;