trifluoro-acetic acid 1-ethyl-1-[2-(2-methoxy-phenyl)-ethyl]-allyl ester

Base Information

Chemical Name:trifluoro-acetic acid 1-ethyl-1-[2-(2-methoxy-phenyl)-ethyl]-allyl ester
CAS No.:243462-26-2
Molecular Formula:C₁₆H₁₉F₃O₃
Molecular Weight:316.32
Hs Code.:

Synonyms:trifluoro-acetic acid 1-ethyl-1-[2-(2-methoxy-phenyl)-ethyl]-allyl ester

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Chemical Property of trifluoro-acetic acid 1-ethyl-1-[2-(2-methoxy-phenyl)-ethyl]-allyl ester

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Technology Process of trifluoro-acetic acid 1-ethyl-1-[2-(2-methoxy-phenyl)-ethyl]-allyl ester

There total 4 articles about trifluoro-acetic acid 1-ethyl-1-[2-(2-methoxy-phenyl)-ethyl]-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 407-25-0
trifluoroacetic anhydride

: 243462-22-8
3-ethyl-5-(2-methoxy-phenyl)-pent-1-en-3-ol

: 243462-26-2
trifluoro-acetic acid 1-ethyl-1-[2-(2-methoxy-phenyl)-ethyl]-allyl ester

Guidance literature:: With pyridine; dmap; In dichloromethane; at 0 ℃; for 12h;
DOI:10.1016/S0022-1139(99)00042-1

Reference yield:

: 135-02-4
ortho-anisaldehyde

: 243462-26-2
trifluoro-acetic acid 1-ethyl-1-[2-(2-methoxy-phenyl)-ethyl]-allyl ester

Guidance literature:: Multi-step reaction with 4 steps

2.1: H₂

3.1: Mg / tetrahydrofuran

3.2: 87 percent / tetrahydrofuran / 1 h

4.1: 93 percent / pyridine; DMAP / CH₂Cl₂ / 12 h / 0 °C

With pyridine; dmap; hydrogen; magnesium; In tetrahydrofuran; dichloromethane; 1.1: aldol condensation / 2.1: Catalytic hydrogenation / 3.1: Metallation / 3.2: Grignard reaction / 4.1: Acylation;
DOI:10.1016/S0022-1139(99)00042-1

Reference yield:

: 91496-03-6
(E)-1-(2-Methoxy-phenyl)-pent-1-en-3-one

: 243462-26-2
trifluoro-acetic acid 1-ethyl-1-[2-(2-methoxy-phenyl)-ethyl]-allyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: H₂

2.1: Mg / tetrahydrofuran

2.2: 87 percent / tetrahydrofuran / 1 h

3.1: 93 percent / pyridine; DMAP / CH₂Cl₂ / 12 h / 0 °C

With pyridine; dmap; hydrogen; magnesium; In tetrahydrofuran; dichloromethane; 1.1: Catalytic hydrogenation / 2.1: Metallation / 2.2: Grignard reaction / 3.1: Acylation;
DOI:10.1016/S0022-1139(99)00042-1