S-phenyl N-(tert-butoxycarbonyl)-11-aminoundecanethioate

Base Information

Chemical Name:S-phenyl N-(tert-butoxycarbonyl)-11-aminoundecanethioate
CAS No.:1359015-00-1
Molecular Formula:C₂₂H₃₅NO₃S
Molecular Weight:393.591
Hs Code.:

Synonyms:S-phenyl N-(tert-butoxycarbonyl)-11-aminoundecanethioate

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Chemical Property of S-phenyl N-(tert-butoxycarbonyl)-11-aminoundecanethioate

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Technology Process of S-phenyl N-(tert-butoxycarbonyl)-11-aminoundecanethioate

There total 3 articles about S-phenyl N-(tert-butoxycarbonyl)-11-aminoundecanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 10436-25-6
11-(tert-butoxycarbonylamino)undecanoic acid

: 108-98-5
thiophenol

: 1359015-00-1
S-phenyl N-(tert-butoxycarbonyl)-11-aminoundecanethioate

Guidance literature:: With dicyclohexyl-carbodiimide; In ethyl acetate; at 20 ℃; for 14h; Inert atmosphere;
DOI:10.1021/ol203399x

Reference yield:

: 2432-99-7,25587-80-8,84029-94-7
11-aminoundecanoic acid

: 1359015-00-1
S-phenyl N-(tert-butoxycarbonyl)-11-aminoundecanethioate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water; tert-butyl alcohol / 18 h / Inert atmosphere

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 6 h / Inert atmosphere

With dmap; dicyclohexyl-carbodiimide; sodium hydroxide; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.bmc.2011.07.047

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1359015-00-1
S-phenyl N-(tert-butoxycarbonyl)-11-aminoundecanethioate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water; tert-butyl alcohol / 18 h / Inert atmosphere

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 6 h / Inert atmosphere

With dmap; dicyclohexyl-carbodiimide; sodium hydroxide; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.bmc.2011.07.047