5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁴-benzoyl deoxycytidine

Base Information

Chemical Name:5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁴-benzoyl deoxycytidine
CAS No.:945623-53-0
Molecular Formula:C₄₁H₄₅N₃O₆Si
Molecular Weight:703.91
Hs Code.:

5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N<sup>4</sup>-benzoyl deoxycytidine

Synonyms:5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁴-benzoyl deoxycytidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁴-benzoyl deoxycytidine

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Technology Process of 5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁴-benzoyl deoxycytidine

There total 3 articles about 5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁴-benzoyl deoxycytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 912558-79-3
1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl chloride

: 4836-13-9
N₄-benzoyl-2'-deoxycytidine

: 945623-53-0
5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁴-benzoyl deoxycytidine

Guidance literature:: With dmap; TEA; In pyridine; for 16h;
DOI:10.1246/cl.2007.768

Reference yield:

: 18395-90-9
Di-tert-butyldichlorosilane

: 945623-53-0
5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁴-benzoyl deoxycytidine

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NaOH / pyridine; methanol / 2 h / 20 °C

2: 91 percent / DMAP; TEA / pyridine / 16 h

With dmap; sodium hydroxide; TEA; In pyridine; methanol;
DOI:10.1246/cl.2007.768

Reference yield:

: 24463-15-8
1-pyrenemethanol

: 945623-53-0
5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁴-benzoyl deoxycytidine

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NaOH / pyridine; methanol / 2 h / 20 °C

2: 91 percent / DMAP; TEA / pyridine / 16 h

With dmap; sodium hydroxide; TEA; In pyridine; methanol;
DOI:10.1246/cl.2007.768