Au(C₄H₉)2C₆H₃C₂₀H₂N₄(C₂H₅)4(CH₃)4C₆H₄I⁽¹⁺⁾*BF₄^(1-)=Au(C₄H₉)2C₆H₃C₂₀H₂N₄(C₂H₅)4(CH₃)4C₆H₄IBF₄

Base Information

• Chemical Name: Au(C₄H₉)2C₆H₃C₂₀H₂N₄(C₂H₅)4(CH₃)4C₆H₄I⁽¹⁺⁾*BF₄^(1-)=Au(C₄H₉)2C₆H₃C₂₀H₂N₄(C₂H₅)4(CH₃)4C₆H₄IBF₄
• CAS No.: 879417-15-9
• Molecular Formula: BF₄*C₅₂H₅₉AuIN₄
• Molecular Weight: 1150.74

Synonyms:Au(C₄H₉)2C₆H₃C₂₀H₂N₄(C₂H₅)4(CH₃)4C₆H₄I⁽¹⁺⁾*BF₄^(1-)=Au(C₄H₉)2C₆H₃C₂₀H₂N₄(C₂H₅)4(CH₃)4C₆H₄IBF₄

Chemical Property of Au(C₄H₉)2C₆H₃C₂₀H₂N₄(C₂H₅)4(CH₃)4C₆H₄I⁽¹⁺⁾*BF₄^(1-)=Au(C₄H₉)2C₆H₃C₂₀H₂N₄(C₂H₅)4(CH₃)4C₆H₄IBF₄

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Technology Process of Au(C₄H₉)2C₆H₃C₂₀H₂N₄(C₂H₅)4(CH₃)4C₆H₄I⁽¹⁺⁾*BF₄^(1-)=Au(C₄H₉)2C₆H₃C₂₀H₂N₄(C₂H₅)4(CH₃)4C₆H₄IBF₄

There total 1 articles about Au(C₄H₉)2C₆H₃C₂₀H₂N₄(C₂H₅)4(CH₃)4C₆H₄I⁽¹⁺⁾*BF₄^(1-)=Au(C₄H₉)2C₆H₃C₂₀H₂N₄(C₂H₅)4(CH₃)4C₆H₄IBF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

Au(tetrahydrothiophene)2BF4 + (C4H9)2C6H3C20H4N4(C2H5)4(CH3)4C6H4I → Au(C4H9)2C6H3C20H2N4(C2H5)4(CH3)4C6H4I(1+)*BF4(1-)=Au(C4H9)2C6H3C20H2N4(C2H5)4(CH3)4C6H4IBF4 (879417-15-9)

Guidance literature:

With 2,6-lutidine; In chloroform; ligand, Au-complex and 2,6-lutidine in CHCl3 was heated to reflux for 1 h; solvent was evapd., residue was dissolved in CH2Cl2, column chromy. on Al2O3 with CH2Cl2, eluted with MeOH/CH2Cl2, recrystd. from CH2Cl2/hexane;

DOI:10.1021/ja003820k

Reference yield: 26.0%

Zn((C4H9)2C6H3C20H2N4(C2H5)4(CH3)4)C6H4C2C6H4C2H (239105-98-7) + Au(C4H9)2C6H3C20H2N4(C2H5)4(CH3)4C6H4I(1+)*BF4(1-)=Au(C4H9)2C6H3C20H2N4(C2H5)4(CH3)4C6H4IBF4 (879417-15-9) → AuZn((C4H9)2C6H3C20H2N4(C2H5)4(CH3)4)2C6H4C2C6H4C2C6H4(1+)*BF4(1-)

Guidance literature:

With AsPh₃; Et₃N; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In chloroform; Pd-complex and AsPh3 were added under Ar to soln. of Zn- and Au-complexes in CHCl3/Et3N, stirred at 40°C overnight; solvent was evapd., column chromy. on Al2O3 with CH2Cl2, eluted with MeOH/CH2Cl2, evapd., triturated with toluene, recrystd. from CH2Cl2/hexane;

DOI:10.1021/ja003820k

Reference yield: 13.0%

4-ethynyl-1-[[zinc(II) porphyrinyl]phenylethynyl]bicyclo[2.2.2]-octane (307334-83-4) + Au(C4H9)2C6H3C20H2N4(C2H5)4(CH3)4C6H4I(1+)*BF4(1-)=Au(C4H9)2C6H3C20H2N4(C2H5)4(CH3)4C6H4IBF4 (879417-15-9) + zinc(II) chloride (7646-85-7,24359-56-6) → AuZn((C4H9)2C6H3C20H2N4(C2H5)4(CH3)4)2C6H4C2C8H12C2C6H4(1+)*BF4(1-)

Guidance literature:

With NaI; NH₄Cl; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In further solvent(s); Pd-complex, ZnCl2 and NaI were added under Ar to soln. of Zn- and Au-complexes in piperidine, stirred at 80°C for 6 d; poured into CH2Cl2, washed with aq. NH4Cl, aq. phase was extd. with CH2Cl2, dried over Na2SO4, evapd., chromy. on Al2O3 with CH2Cl2, eluted withMeOH/CH2Cl2, evapd., triturated with toluene, recrystd. from CH2Cl2/hex ane;

DOI:10.1021/ja003820k

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